Technology Process of 1-Pentanone, 1-(2-iodophenyl)-
There total 2 articles about 1-Pentanone, 1-(2-iodophenyl)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-iodo-succinimide; silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper diacetate;
In
1,2-dichloro-ethane;
at 120 ℃;
for 20h;
Sealed tube;
DOI:10.1039/d0cc02941f
- Guidance literature:
-
Multistep reaction;
(i)Et2O, THF, (ii) CrO3, H2SO4, H2O;
DOI:10.1021/jo00971a015
- Guidance literature:
-
trifluoroacetic acid-methyl ester;
With
sodium hydride;
In
tetrahydrofuran;
at 20 ℃;
for 0.166667h;
Inert atmosphere;
Schlenk technique;
1-(2-iodophenyl)pentan-1-one;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 3h;
Inert atmosphere;
Schlenk technique;
With
hydrogenchloride;
In
tetrahydrofuran; water;
at 0 ℃;
for 0.25h;
Inert atmosphere;
Schlenk technique;
DOI:10.1016/j.tet.2014.05.017
