1-Chloro-N,N-dimethyl-N',N'-bis(trimethylsilyl)boranediamine

Base Information

• Chemical Name: 1-Chloro-N,N-dimethyl-N',N'-bis(trimethylsilyl)boranediamine
• CAS No.: 32882-72-7
• Molecular Formula: C8H24BClN2Si2
• Molecular Weight: 250.727
• DSSTox Substance ID: DTXSID70533219
• Wikidata: Q82406383

Synonyms:32882-72-7;DTXSID70533219;1-Chloro-N,N-dimethyl-N',N'-bis(trimethylsilyl)boranediamine

Chemical Property of 1-Chloro-N,N-dimethyl-N',N'-bis(trimethylsilyl)boranediamine

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 250.1259597
• Heavy Atom Count: 14
• Complexity: 175

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: B(N(C)C)(N([Si](C)(C)C)[Si](C)(C)C)Cl

Technology Process of 1-Chloro-N,N-dimethyl-N',N'-bis(trimethylsilyl)boranediamine

There total 2 articles about 1-Chloro-N,N-dimethyl-N',N'-bis(trimethylsilyl)boranediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

{(CH3)3Si}2NB{N(CH3)2}2 (32882-73-8) → Bis(trimethylsilyl)aminochlorodimethylaminoboran (32882-72-7) + N,N-dimethylammonium chloride (506-59-2)

Guidance literature:

With HCl; In toluene; sepn. of dimethylamine hydrochloride and toluene, distn.;

Reference yield: 16.0%

Cl2B-N(CH3)2*N(CH3)3 + 1,1,1,3,3,3-hexamethyl-disilazane (999-97-3) → Bis(trimethylsilyl)aminochlorodimethylaminoboran (32882-72-7) + trimethylamine hydrochloride (593-81-7)

Guidance literature:

In benzene; stirring for 1 week in dry benzene; sepn. of trimethylamine hydrochloride and benzene;

upstream raw materials:

1,1,1,3,3,3-hexamethyl-disilazane

{(CH₃)3Si}2NB{N(CH₃)2}2

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