3-Chloro-9-methylcarbazole

Base Information

Chemical Name:3-Chloro-9-methylcarbazole
CAS No.:33268-90-5
Molecular Formula:C13H10ClN
Molecular Weight:215.682
Hs Code.:
DSSTox Substance ID:DTXSID10369559
Nikkaji Number:J848.344B
Wikidata:Q82156715

Synonyms:3-chloro-9-methylcarbazole;9H-Carbazole, 3-chloro-9-methyl-;33268-90-5;9-methyl-3-chlorocarbazole;SCHEMBL1921474;3-chloro-9-methyl-9H-carbazole;DTXSID10369559;CCG-248777

Suppliers and Price of 3-Chloro-9-methylcarbazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 3-Chloro-9-methylcarbazole

Chemical Property:

XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:215.0501770
Heavy Atom Count:15
Complexity:243

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C2=C(C=C(C=C2)Cl)C3=CC=CC=C31

Technology Process of 3-Chloro-9-methylcarbazole

There total 5 articles about 3-Chloro-9-methylcarbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13278-35-8
2-(4-chloroanilino)benzoic acid

: 1484-12-4
N-methylcarbazole

: 33268-90-5
3-chloro-9-methyl-9H-carbazole

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide / 2 h / 20 °C

2: potassium hydroxide / methanol; water / 12 h / Reflux

3: pyridine / dimethylsulfoxide-d6 / 48 h / Irradiation

With pyridine; sodium hydride; potassium hydroxide; In methanol; dimethylsulfoxide-d6; water; N,N-dimethyl-formamide;
DOI:10.1039/d0gc02789h

Reference yield:

: 88-65-3
2-bromobenzoic-acid

: 1484-12-4
N-methylcarbazole

: 33268-90-5
3-chloro-9-methyl-9H-carbazole

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate; copper(I) oxide; copper / 2-methoxy-ethanol / 24 h / 130 °C / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide / 2 h / 20 °C

3: potassium hydroxide / methanol; water / 12 h / Reflux

4: pyridine / dimethylsulfoxide-d6 / 48 h / Irradiation

With pyridine; copper(I) oxide; copper; sodium hydride; potassium carbonate; potassium hydroxide; In methanol; dimethylsulfoxide-d6; 2-methoxy-ethanol; water; N,N-dimethyl-formamide;
DOI:10.1039/d0gc02789h

Reference yield:

: 106-47-8
4-chloro-aniline

: 1484-12-4
N-methylcarbazole

: 33268-90-5
3-chloro-9-methyl-9H-carbazole

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate; copper(I) oxide; copper / 2-methoxy-ethanol / 24 h / 130 °C / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide / 2 h / 20 °C

3: potassium hydroxide / methanol; water / 12 h / Reflux

4: pyridine / dimethylsulfoxide-d6 / 48 h / Irradiation

With pyridine; copper(I) oxide; copper; sodium hydride; potassium carbonate; potassium hydroxide; In methanol; dimethylsulfoxide-d6; 2-methoxy-ethanol; water; N,N-dimethyl-formamide;
DOI:10.1039/d0gc02789h