Cycloheptanone, phenylhydrazone

Base Information

• Chemical Name: Cycloheptanone, phenylhydrazone
• CAS No.: 3349-69-7
• Molecular Formula: C13H18N2
• Molecular Weight: 202.299
• Mol file: 3349-69-7.mol

Synonyms:

Chemical Property of Cycloheptanone, phenylhydrazone

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cycloheptanone, phenylhydrazone

There total 3 articles about Cycloheptanone, phenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

→ 1-cycloheptylidene-2-phenylhydrazine (3349-69-7)

Guidance literature:

With sodium methylate; In toluene; for 3h; Reflux; Dean-Stark;

Reference yield: 85.0%

cycloheptanol (502-41-0) + phenylhydrazine (100-63-0) → 1-cycloheptylidene-2-phenylhydrazine (3349-69-7)

Guidance literature:

cycloheptanol; With chromium(VI) oxide; silica gel; In tert-butyl alcohol; for 0.166667h;

phenylhydrazine; In tert-butyl alcohol; for 0.166667h;

DOI:10.1081/SCC-200058009

Reference yield:

phenylhydrazine (100-63-0) + cycloheptanone (502-42-1) → 1-cycloheptylidene-2-phenylhydrazine (3349-69-7)

Guidance literature:

With acetic acid; for 0.25h; Ambient temperature;

DOI:10.1055/s-1990-27022

upstream raw materials:

phenylhydrazine

cycloheptanone

cycloheptanol

Downstream raw materials:

2-phenyl-2,4,5,6,7,8-hexahydro-cyclohepta[1,2,3]diazarsole

2-formyl-1-phenylhydrazine

cycloheptanone

3-Phenyl-5,6,7,8,9,10-hexahydro-[1,2,4]triazolo[1,5-a]azocin-2-one