1,1'-[(4-Methylphenyl)methylene]dipiperidine

Base Information

• Chemical Name: 1,1'-[(4-Methylphenyl)methylene]dipiperidine
• CAS No.: 35287-01-5
• Molecular Formula: C18H28N2
• Molecular Weight: 272.434
• DSSTox Substance ID: DTXSID30560243
• Wikidata: Q82443255
• Mol file: 35287-01-5.mol

Synonyms:35287-01-5;1,1'-[(4-Methylphenyl)methylene]dipiperidine;DTXSID30560243

Chemical Property of 1,1'-[(4-Methylphenyl)methylene]dipiperidine

Chemical Property:

• XLogP3: 4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 272.225248902
• Heavy Atom Count: 20
• Complexity: 253

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC=C(C=C1)C(N2CCCCC2)N3CCCCC3

Technology Process of 1,1'-[(4-Methylphenyl)methylene]dipiperidine

There total 3 articles about 1,1'-[(4-Methylphenyl)methylene]dipiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

1-(trimethylsilyl)piperidine (3768-56-7) + 4-methyl-benzaldehyde (104-87-0) → bis(piperidino)(4-methylphenyl)methane (35287-01-5) + Hexamethyldisiloxane (107-46-0)

Guidance literature:

With bromine; trimethylsilyl trifluoromethanesulfonate; In tetrachloromethane; for 2h; Ambient temperature;

Reference yield: 47.6%

piperidine (110-89-4) + 1-(Bromo-p-tolyl-methyl)-pyridinium; bromide (113700-15-5) → bis(piperidino)(4-methylphenyl)methane (35287-01-5)

Guidance literature:

In chloroform; at 0 ℃; for 4h;

DOI:10.1021/jo00281a021

Reference yield:

→ bis(piperidino)(4-methylphenyl)methane (35287-01-5)

Guidance literature:

4-Methyl-benzaldehyd, Piperidin;

upstream raw materials:

piperidine

1-(Bromo-p-tolyl-methyl)-pyridinium; bromide

1-(trimethylsilyl)piperidine

4-methyl-benzaldehyde

Downstream raw materials:

piperidine

N,N-piperidyl-1-p-tolylmethanamine

4-(4-methylphenyl)-4-piperidino-1-butene

N-(4,4'-dimethyl)benzhydrylpiperidine

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