(3-Chloro-2-methylpropyl)dimethoxymethylsilane

Base Information

• Chemical Name: (3-Chloro-2-methylpropyl)dimethoxymethylsilane
• CAS No.: 18244-20-7
• Molecular Formula: C7H17 Cl O2 Si
• Molecular Weight: 196.749
• European Community (EC) Number: 242-117-1
• DSSTox Substance ID: DTXSID10864817
• Nikkaji Number: J266.072E
• Mol file: 18244-20-7.mol

Synonyms:(3-Chloro-2-methylpropyl)dimethoxymethylsilane;18244-20-7;(3-chloro-2-methylpropyl)-dimethoxy-methylsilane;EINECS 242-117-1;SCHEMBL731627;DTXSID10864817;2-methylchloropropyl methyldimethoxysilane;3-chloro-2-methylpropylmethyldimethoxysilane;3-Chloro-2-methylpropyldimethoxy(methyl)silane

Chemical Property of (3-Chloro-2-methylpropyl)dimethoxymethylsilane

Chemical Property:

• Vapor Pressure: 0.334mmHg at 25°C
• Boiling Point: 206.8°Cat760mmHg
• Flash Point: 67°C
• PSA: 18.46000
• Density: 0.963g/cm³
• LogP: 2.22610
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 5
• Exact Mass: 196.0686340
• Heavy Atom Count: 11
• Complexity: 107

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C[Si](C)(OC)OC)CCl

Technology Process of (3-Chloro-2-methylpropyl)dimethoxymethylsilane

There total 2 articles about (3-Chloro-2-methylpropyl)dimethoxymethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dichloro(3-chloro-2-methylpropyl)methylsilane (1628-11-1) + methanol (67-56-1) → 3-chloro-2-methylpropyl(methyldimethoxysilane) (18244-20-7)

Guidance literature:

DOI:10.1021/ja01499a031

Reference yield:

(dimethoxy)methylsilane (16881-77-9) + 3-Chloro-2-methylpropene (563-47-3) → 3-chloro-2-methylpropyl(methyldimethoxysilane) (18244-20-7)

Guidance literature:

With tert.-butylhydroperoxide; rhodium(III) chloride hydrate; In methanol; at 58 - 80 ℃;

Reference yield:

3-chloro-2-methylpropyl(methyldimethoxysilane) (18244-20-7) → 2-(2-methoxy-2,4-dimethyl-[1,2]azasilolidin-1-yl)-ethylamine (18441-77-5)

Guidance literature:

Multi-step reaction with 2 steps

2: (heating)

DOI:10.1021/jo00820a011

upstream raw materials:

dichloro(3-chloro-2-methylpropyl)methylsilane

methanol

(dimethoxy)methylsilane

3-Chloro-2-methylpropene

Downstream raw materials:

N-[3-(dimethoxy-methyl-silanyl)-2-methyl-propyl]-ethane-1,2-diamine

2-(2-methoxy-2,4-dimethyl-[1,2]azasilolidin-1-yl)-ethylamine

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