3-Butenoic acid, 2,3-dimethyl-

Base Information

Chemical Name:3-Butenoic acid, 2,3-dimethyl-
CAS No.:36598-04-6
Molecular Formula:C6H10O2
Molecular Weight:114.144
Hs Code.:
DSSTox Substance ID:DTXSID80451995
Nikkaji Number:J2.827.161A
Mol file:36598-04-6.mol

Synonyms:2,3-dimethylbut-3-enoic Acid;36598-04-6;2,3-Dimethyl-3-butenoic acid;3-Butenoic acid, 2,3-dimethyl-;starbld0039837;SCHEMBL965170;DTXSID80451995;AKOS006379375

Suppliers and Price of 3-Butenoic acid, 2,3-dimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 3-Butenoic acid, 2,3-dimethyl-

Chemical Property:

XLogP3:1.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:114.068079557
Heavy Atom Count:8
Complexity:116

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C(=C)C)C(=O)O

Technology Process of 3-Butenoic acid, 2,3-dimethyl-

There total 5 articles about 3-Butenoic acid, 2,3-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: bis(η5-cyclopentadienyl)(η3-1,2-dimethylallyl)titanium

: 1271-19-8
bis(cyclopentadienyl)titanium dichloride

: 36598-04-6
2,3-dimethyl-3-butenoic acid

Guidance literature:: With hydrogenchloride; air; carbon dioxide; In diethyl ether; Passing of gaseous CO2 through Et2O soln. of Ti-compd. (Ar) for 1 h, hydrolysis with aq. HCl and then bubbling of air into react. mixt. for 15 min.; Collecting of pptd. crystals of Cp2TiCl2 by filtn., addn. of aq. NaOH, sepn. of org. layer and discarding. Extn. of aq. layer with ether, discarding, addn. of concd. HCl, extn. with ether, drying, concn. in vac. Purifn. by trap-to-trap distn., (1)H NMR.;
DOI:10.1016/0020-1693(94)03904-6

Reference yield:

: 124-38-9,18923-20-1
carbon dioxide

: 78-79-5,9003-31-0
isoprene

: 10276-09-2
2,2-dimethyl-but-3-enoic acid

: 36598-04-6
2,3-dimethyl-3-butenoic acid

: 79-31-2
isobutyric Acid

: 153580-51-9
3,7-dimethyl-1,7-octadiene-3-carboxylic acid

Guidance literature:: With bis(triphenylphosphine)nickel(II) chloride; sulfuric acid; isopropylmagnesium chloride; Yield given. Multistep reaction. Yields of byproduct given;

Reference yield:

: 124-38-9,18923-20-1
carbon dioxide

: 78-79-5,9003-31-0
isoprene

: 10276-09-2
2,2-dimethyl-but-3-enoic acid

: 36598-04-6
2,3-dimethyl-3-butenoic acid

: 79-31-2
isobutyric Acid

: 3,6-dimethyl-1,7-octadiene-3-carboxylic acid

Guidance literature:: With [nickel(II)(pyridine)4(chloride)2]; sulfuric acid; isopropylmagnesium chloride; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;