2-Fluoro-4-Nitrothioanisole

Base Information

• Chemical Name: 2-Fluoro-4-Nitrothioanisole
• CAS No.: 372121-91-0
• Molecular Formula: C7H6FNO2S
• Molecular Weight: 187.195
• Mol file: 372121-91-0.mol

Synonyms:2-Fluoro-4-nitrothioanisole;3-fluoro-4-methylsulfanylnitrobenzene;2-fluoro-1-methylthio-4-nitrobenzene;2-fluoro-1-methylsulfanyl-4-nitro-benzene;

Chemical Property of 2-Fluoro-4-Nitrothioanisole

Chemical Property:

• PSA: 71.12000
• LogP: 2.97900

Purity/Quality:

97% ^*data from raw suppliers

2-FLUORO-4-NITROTHIOANISOLE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Fluoro-4-Nitrothioanisole

There total 1 articles about 2-Fluoro-4-Nitrothioanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

3,4-difluoronitrobenzene (369-34-6) + sodium thiomethoxide (5188-07-8) → (2-fluoro-4-nitrophenyl)(methyl)sulfone (372121-91-0)

Guidance literature:

In tetrahydrofuran; DMF (N,N-dimethyl-formamide); at 20 ℃; for 6.16667h;

Reference yield: 97.0%

(2-fluoro-4-nitrophenyl)(methyl)sulfone (372121-91-0) → 3-fluoro-4-(methylthio)benzeneamine (20901-69-3)

Guidance literature:

With water; iron; acetic acid; for 2h;

Reference yield: 92.8%

(2-fluoro-4-nitrophenyl)(methyl)sulfone (372121-91-0) → (2-fluoro-4-nitrophenyl)(imino)(methyl)-16-sulfanone (851008-59-8)

Guidance literature:

With [bis(acetoxy)iodo]benzene; ammonium carbamate; In methanol; at 20 ℃; for 3h;

upstream raw materials:

3,4-difluoronitrobenzene

sodium thiomethoxide

Downstream raw materials:

3-fluoro-4-(methylthio)benzeneamine

C₇H₆FNO₃S

N-(2-(3-fluoro-4-(methylsulfonyl)phenoxy)ethyl)-1-(3-isopropyl-1,2,4-oxadiazol-5-yl)-N-methylpiperidine-4-amine

N-(2-(3-fluoro-4-(methylsulfonyl)phenoxy)ethyl)-1-(3-isopropyl-1,2,4-oxadiazol-5-yl)-N-methylpiperidine-4-amine trifluoroacetate

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