Hydrazinecarboxylic acid, phenyl[1-phenyl-2-(phenylthio)ethylidene]-, ethyl ester, (2Z)-

Base Information

Chemical Name:Hydrazinecarboxylic acid, phenyl[1-phenyl-2-(phenylthio)ethylidene]-, ethyl ester, (2Z)-
CAS No.:381730-32-1
Molecular Formula:C23H22N2O2S
Molecular Weight:390.506
Hs Code.:
Mol file:381730-32-1.mol

Synonyms:

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Chemical Property of Hydrazinecarboxylic acid, phenyl[1-phenyl-2-(phenylthio)ethylidene]-, ethyl ester, (2Z)-

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Technology Process of Hydrazinecarboxylic acid, phenyl[1-phenyl-2-(phenylthio)ethylidene]-, ethyl ester, (2Z)-

There total 6 articles about Hydrazinecarboxylic acid, phenyl[1-phenyl-2-(phenylthio)ethylidene]-, ethyl ester, (2Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 111709-02-5
benzaldehyde N-(carboethoxy)-N-phenylhydrazone

: 381730-32-1
N-phenyl-N'-(1-phenyl-2-phenylsulfanyl-ethylidene)-hydrazinecarboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / HCl / H₂O; ethanol / 40 °C

2: trifluoroacetic acid; toluene

With hydrogenchloride; In ethanol; water; toluene; trifluoroacetic acid;
DOI:10.1021/ol0165645

Reference yield:

: 16222-10-9
1-phenyl-2-(phenylthio)ethanone

: 381730-32-1
N-phenyl-N'-(1-phenyl-2-phenylsulfanyl-ethylidene)-hydrazinecarboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid

2: n-BuLi / -78 °C

With n-butyllithium; In acetic acid;
DOI:10.1021/ol0165645

Reference yield:

: 100-63-0
phenylhydrazine

: 381730-32-1
N-phenyl-N'-(1-phenyl-2-phenylsulfanyl-ethylidene)-hydrazinecarboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid

2: n-BuLi / -78 °C

With n-butyllithium; In acetic acid;
DOI:10.1021/ol0165645