M-TyraMine HydrobroMide

Base Information

• Chemical Name: M-TyraMine HydrobroMide
• CAS No.: 38449-59-1
• Molecular Formula: C8H11NO.BrH
• Molecular Weight: 218.093
• Mol file: 38449-59-1.mol

Synonyms:3-(2-aminoethyl)phenol hydrobromide;2-(3-hydroxyphenyl)-1-aminoethane hydrobromide;3-hydroxyphenethylamine hydrobromide;m-Tyramine hydrobromide;

Chemical Property of M-TyraMine HydrobroMide

Chemical Property:

• Melting Point: 115-118°C
• PSA: 46.25000
• LogP: 2.55180
• Storage Temp.: Refrigerator
• Solubility.: DMSO (Slightly), Methanol (Slightly)

Purity/Quality:

99% ^*data from raw suppliers

m-TyramineHydrobromide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: Brain microsomes were able to metabolize tyramine to dopamine.

Technology Process of M-TyraMine HydrobroMide

There total 4 articles about M-TyraMine HydrobroMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-(3-methoxyphenyl)-1-ethanamine (2039-67-0) → 2-(3-hydroxyphenyl)ethylamine hydrobromide (38449-59-1)

Guidance literature:

With hydrogen bromide; In water; for 1.5h; Inert atmosphere; Reflux;

DOI:10.1002/chem.201102018

Reference yield:

3-methoxyphenylacetonitrile (19924-43-7) → 2-(3-hydroxyphenyl)ethylamine hydrobromide (38449-59-1)

Guidance literature:

Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride; aluminum (III) chloride / tetrahydrofuran; diethyl ether / 20 °C / Inert atmosphere

2: hydrogen bromide / water / 1.5 h / Inert atmosphere; Reflux

With aluminum (III) chloride; lithium aluminium tetrahydride; hydrogen bromide; In tetrahydrofuran; diethyl ether; water;

DOI:10.1002/chem.201102018

Reference yield:

1-bromomethyl-3-methoxybenzene (874-98-6) → 2-(3-hydroxyphenyl)ethylamine hydrobromide (38449-59-1)

Guidance literature:

Multi-step reaction with 3 steps

1: ethanol; water / 3 h / Inert atmosphere; Reflux

2: lithium aluminium tetrahydride; aluminum (III) chloride / tetrahydrofuran; diethyl ether / 20 °C / Inert atmosphere

3: hydrogen bromide / water / 1.5 h / Inert atmosphere; Reflux

With aluminum (III) chloride; lithium aluminium tetrahydride; hydrogen bromide; In tetrahydrofuran; diethyl ether; ethanol; water;

DOI:10.1002/chem.201102018

upstream raw materials:

2-(3-methoxyphenyl)-1-ethanamine

3-methoxyphenylacetonitrile

1-bromomethyl-3-methoxybenzene

1-methoxy-3-methyl-benzene

Downstream raw materials:

rac-6-hydroxy-1,2,3,4-tetrahydroisoquinoline-1-carboxylic acid

ethyl (1SR)-6-hydroxy-1,2,3,4-tetrahydroisoquinoline-1-carboxylate

1,2,3,4-Tetrahydro-6-hydroxy-1-isoquinolinecarboxylic acid methyl ester

N⁽¹⁾-(4-butylphenyl)-N⁽²⁾-(3-hydroxyphenethyl)phthalamide

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