Technology Process of Benzoic acid, 2-benzoyl-1,2-bis(phenylmethoxy)hydrazide
There total 4 articles about Benzoic acid, 2-benzoyl-1,2-bis(phenylmethoxy)hydrazide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutylammonium acetate;
In
methanol; acetonitrile;
at 20 ℃;
for 4h;
Electrochemical reaction;
DOI:10.1021/acs.joc.1c01294
- Guidance literature:
-
Multi-step reaction with 3 steps
1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C
2: potassium carbonate / ethyl acetate; water / 4 h / 0 °C
3: tetrabutylammonium acetate / acetonitrile; methanol / 4 h / 20 °C / Electrochemical reaction
With
oxalyl dichloride; tetrabutylammonium acetate; potassium carbonate; N,N-dimethyl-formamide;
In
methanol; dichloromethane; water; ethyl acetate; acetonitrile;
DOI:10.1021/acs.joc.1c01294
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / ethyl acetate; water / 4 h / 0 °C
2: tetrabutylammonium acetate / acetonitrile; methanol / 4 h / 20 °C / Electrochemical reaction
With
tetrabutylammonium acetate; potassium carbonate;
In
methanol; water; ethyl acetate; acetonitrile;
DOI:10.1021/acs.joc.1c01294
