2-Cyanobenzyl acetate

Base Information

• Chemical Name: 2-Cyanobenzyl acetate
• CAS No.: 38866-59-0
• Molecular Formula: C10H9NO2
• Molecular Weight: 175.18400
• Hs Code.: 2926907090
• Mol file: 38866-59-0.mol

Synonyms:(2-Cyan-benzyl)-acetat;Essigsaeure-2-cyanobenzylester;2-Acetoxymethyl-benzonitril;2-acetoxymethyl-benzonitrile;

Chemical Property of 2-Cyanobenzyl acetate

Chemical Property:

• PSA: 50.09000
• LogP: 1.62138
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

2-CyanobenzylAcetate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Cyanobenzyl acetate

There total 4 articles about 2-Cyanobenzyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium acetate (127-09-3) + 2-cyanobenzyl chloride (612-13-5) → 2-cyanobenzyl acetate (38866-59-0)

Guidance literature:

at 100 - 110 ℃;

Reference yield:

acetic acid (64-19-7,77671-22-8) + 2-(bromomethyl)benzonitrile (22115-41-9) → 2-cyanobenzyl acetate (38866-59-0)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

DOI:10.1039/c4cc04072d

Reference yield:

2-Methylbenzonitrile (529-19-1) → 2-cyanobenzyl acetate (38866-59-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 120 - 130 °C / Irradiation_.durch Chlorierung

2: 100 - 110 °C

upstream raw materials:

sodium acetate

2-cyanobenzyl chloride

silver(I) acetate

2-(bromomethyl)benzonitrile

Downstream raw materials:

(Z)-2-(1-acetamido-4-(triisopropylsilyl)but-1-en-3-yn-1-yl)benzyl acetate

C₁₃H₁₅NO₃

2-(hydroxymethyl)benzenecorbonitrile

Refernces