1H-Isoindole-1,3(2H)-dione, 2-[[1,2,3,6-tetrahydro-1-[(4-methoxyphenyl)methyl]-4-[(trimethylsilyl)oxy]- 2-pyridinyl]methyl]-

Base Information

Chemical Name:1H-Isoindole-1,3(2H)-dione, 2-[[1,2,3,6-tetrahydro-1-[(4-methoxyphenyl)methyl]-4-[(trimethylsilyl)oxy]- 2-pyridinyl]methyl]-
CAS No.:390426-71-8
Molecular Formula:C25H30N2O4Si
Molecular Weight:450.61
Hs Code.:
Mol file:390426-71-8.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-Isoindole-1,3(2H)-dione, 2-[[1,2,3,6-tetrahydro-1-[(4-methoxyphenyl)methyl]-4-[(trimethylsilyl)oxy]- 2-pyridinyl]methyl]-

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Technology Process of 1H-Isoindole-1,3(2H)-dione, 2-[[1,2,3,6-tetrahydro-1-[(4-methoxyphenyl)methyl]-4-[(trimethylsilyl)oxy]- 2-pyridinyl]methyl]-

There total 4 articles about 1H-Isoindole-1,3(2H)-dione, 2-[[1,2,3,6-tetrahydro-1-[(4-methoxyphenyl)methyl]-4-[(trimethylsilyl)oxy]- 2-pyridinyl]methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2913-97-5
N-phthalimidyl-2-aminoacetaldehyde

: 38053-91-7
2-trimethylsilyloxy-1,3-butadiene

: 2393-23-9
4-methoxy-benzylamine

: 390426-43-4
2-[{1-(4-methoxybenzyl)-4-oxopiperidin-2-yl}methyl]isoindole-1,3-dione

: 390426-71-8
2-(1-(4-methoxy-benzyl)-4-trimethyl-silanyloxy-1,2,3,6-tetrahydro-pyridin-2-ylmethyl)-isoindole-1,3-dione

Guidance literature:: With hydrogenchloride; aluminium trichloride; silica gel; In dichloromethane; water; ethyl acetate;

Reference yield:

: 38053-91-7
2-trimethylsilyloxy-1,3-butadiene

: 2-{2-[(Z)-4-Methoxy-benzylimino]-ethyl}-isoindole-1,3-dione

: 390426-71-8
2-(1-(4-methoxy-benzyl)-4-trimethyl-silanyloxy-1,2,3,6-tetrahydro-pyridin-2-ylmethyl)-isoindole-1,3-dione

Guidance literature:: With aluminium trichloride; In dichloromethane; at -78 - 20 ℃; for 18h;
DOI:10.1081/SCC-120018941

Reference yield:

: 2913-97-5
N-phthalimidyl-2-aminoacetaldehyde

: 390426-71-8
2-(1-(4-methoxy-benzyl)-4-trimethyl-silanyloxy-1,2,3,6-tetrahydro-pyridin-2-ylmethyl)-isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: molecular sieves 4 Angstroem / CH₂Cl₂ / 1 h / 20 °C

2: aluminum chloride / CH₂Cl₂ / 18 h / -78 - 20 °C

With aluminium trichloride; 4 A molecular sieve; In dichloromethane; 2: hetero Diels-Alder reaction;
DOI:10.1081/SCC-120018941