(4-methyl-3-cyclohexen-1-yl)methanol(SALTDATA: FREE)

Base Information

• Chemical Name: (4-methyl-3-cyclohexen-1-yl)methanol(SALTDATA: FREE)
• CAS No.: 39155-38-9
• Molecular Formula: C8H14O
• Molecular Weight: 126.199
• Hs Code.: 2906199090
• Mol file: 39155-38-9.mol

Synonyms:4-methyl-3-cyclohexene-1-methanol;para-methyl-3-cyclohexanetetrahydrobenzyl alcohol;3-cyclohexene-1-methanol,4-methyl;4-methyl-3-cyclohexenylmethanol;4-methylcyclohex-3-enylmethanol;(4-Methyl-3-cyclohexen-1-yl)methanol;

Chemical Property of (4-methyl-3-cyclohexen-1-yl)methanol(SALTDATA: FREE)

Chemical Property:

• Vapor Pressure: 0.223mmHg at 25°C
• Boiling Point: 105 °C(Press: 20 Torr)
• PKA: 14.96±0.10(Predicted)
• PSA: 20.23000
• Density: 0.925±0.06 g/cm3(Predicted)
• LogP: 1.72510

Purity/Quality:

99% ^*data from raw suppliers

(4-methylcyclohex-3-en-1-yl)methanol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (4-methyl-3-cyclohexen-1-yl)methanol(SALTDATA: FREE)

There total 6 articles about (4-methyl-3-cyclohexen-1-yl)methanol(SALTDATA: FREE) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

4-methylcyclohex-3-enecarboxylic acid (4342-60-3) → (4-methylcyclohex-3-en-1-yl)methanol (39155-38-9)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 7h; Heating;

DOI:10.1080/00397919408010239

Reference yield: 80.0%

methyl 4-methyl-3-cyclohexene-1-carboxylate (6493-79-4,5443-14-1) → (4-methylcyclohex-3-en-1-yl)methanol (39155-38-9)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 0 - 20 ℃; for 1h; Schlenk technique;

DOI:10.1021/ja507902z

Reference yield: 73.0%

4-methyl-cyclohex-3-enecarboxylic acid ethyl ester (20292-15-3) → (4-methylcyclohex-3-en-1-yl)methanol (39155-38-9)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1002/hlca.19960790606

upstream raw materials:

4-methyl-cyclohex-3-enecarbaldehyde

4-methylcyclohex-3-enecarboxylic acid

4-methyl-cyclohex-3-enecarboxylic acid ethyl ester

methyl 4-methyl-3-cyclohexene-1-carboxylate

Downstream raw materials:

1-Methyl-4-nitrosooxymethyl-cyclohexene

(trans-4-methylcyclohexyl)methanol

(cis-4-Methyl-cyclohexyl)-methanol

4-methyl-cyclohex-3-enecarbaldehyde