Silane, [[2-(4-bromo-1,2-dihydro-2-benzogermin-2-yl)-1,3,5-benzenetriyl]trimeth ylidyne]hexakis[trimethyl-

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Chemical Name:Silane, [[2-(4-bromo-1,2-dihydro-2-benzogermin-2-yl)-1,3,5-benzenetriyl]trimeth ylidyne]hexakis[trimethyl-
CAS No.:392335-75-0
Molecular Formula:C₃₆H₆₇BrGeSi₆
Molecular Weight:820.935
Hs Code.:

Synonyms:

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Chemical Property of Silane, [[2-(4-bromo-1,2-dihydro-2-benzogermin-2-yl)-1,3,5-benzenetriyl]trimeth ylidyne]hexakis[trimethyl-

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Technology Process of Silane, [[2-(4-bromo-1,2-dihydro-2-benzogermin-2-yl)-1,3,5-benzenetriyl]trimeth ylidyne]hexakis[trimethyl-

There total 3 articles about Silane, [[2-(4-bromo-1,2-dihydro-2-benzogermin-2-yl)-1,3,5-benzenetriyl]trimeth ylidyne]hexakis[trimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 38256-56-3
1-(2-bromo-ethyl)-2-bromomethyl-benzene

: 392335-71-6
2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-1,2-dihydro-2-germanaphthalene

: 392335-75-0
2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-1,2-dihydro-4-bromo-2-germanaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: magnesium; LiAlH₄ / tetrahydrofuran

2: LiAlH₄; catalyst: benzoyl peroxide / tetrahydrofuran; benzene

With magnesium; LiAlH₄; catalyst: benzoyl peroxide; In tetrahydrofuran; benzene;
DOI:10.1021/om020879m

Reference yield:

: 135139-64-9
2,4,6-tris(bis(trimethylsilyl)methyl)phenylgermanium trichloride

: 392335-71-6
2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-1,2-dihydro-2-germanaphthalene

: 392335-75-0
2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-1,2-dihydro-4-bromo-2-germanaphthalene

Guidance literature:: Multi-step reaction with 2 steps

1: magnesium; LiAlH₄ / tetrahydrofuran

2: LiAlH₄; catalyst: benzoyl peroxide / tetrahydrofuran; benzene

With magnesium; LiAlH₄; catalyst: benzoyl peroxide; In tetrahydrofuran; benzene;
DOI:10.1021/om020879m

Reference yield:

: 128-08-5
N-Bromosuccinimide

: 392335-70-5
2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-1,2,3,4-tetrahydro-2-germanaphthalene

: 392335-71-6
2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-1,2-dihydro-2-germanaphthalene

: 392335-75-0
2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-1,2-dihydro-4-bromo-2-germanaphthalene

Guidance literature:: With LiAlH₄; catalyst: benzoyl peroxide; In tetrahydrofuran; benzene; under Ar, benzene soln. was refluxed for 2 h, solvent was removed, THF was added, then LiAlH4 was added at 0°C, and suspn. was stirred for 1 h; aq. NaOH was added at 0°C, suspn. was filtered, hexane was added,solvent was evapd., residue was purified by FCC (hexane), inseparable m ixt.; NMR;
DOI:10.1021/om020879m