Oxolan-2-yl(diphenyl)methanol

Base Information

• Chemical Name: Oxolan-2-yl(diphenyl)methanol
• CAS No.: 25330-02-3
• Molecular Formula: C17H18 O2
• Molecular Weight: 254.329
• NSC Number: 118149
• DSSTox Substance ID: DTXSID60297792
• Mol file: 25330-02-3.mol

Synonyms:25330-02-3;oxolan-2-yl(diphenyl)methanol;diphenyl(tetrahydrofuran-2-yl)methanol;NSC118149;DTXSID60297792;NSC-118149

Chemical Property of Oxolan-2-yl(diphenyl)methanol

Chemical Property:

• Vapor Pressure: 1.37E-07mmHg at 25°C
• Boiling Point: 413.8°C at 760 mmHg
• Flash Point: 188.1°C
• Density: 1.158g/cm³
• XLogP3: 3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 254.130679813
• Heavy Atom Count: 19
• Complexity: 259

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CC(OC1)C(C2=CC=CC=C2)(C3=CC=CC=C3)O

Technology Process of Oxolan-2-yl(diphenyl)methanol

There total 10 articles about Oxolan-2-yl(diphenyl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

7-benzyloxy-5-(2-oxoheptyl)-2,2-diphenylbenzo[1,3]dioxin-4-one (846606-85-7) + tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + methanol (67-56-1) → 4-benzyloxy-2-hydroxy-6-(2-oxoheptyl)benzoic acid methyl ester (846606-89-1) + 1,1-Diphenylmethanol (91-01-0) + 2-(diphenylhydroxymethyl)-tetrahydrofuran (25330-02-3)

Guidance literature:

In tetrahydrofuran; for 5h; Photolysis;

DOI:10.1021/ol047507p

Reference yield: 88.0%

tetrahydrofuran (109-99-9,24979-97-3,77392-70-2) + 1-Methyl-4-((E)-1-methylsulfanyl-prop-1-ene-1-sulfonyl)-benzene (99946-84-6,260547-98-6) → 2-(diphenylhydroxymethyl)-tetrahydrofuran (25330-02-3) + 2-[1-Methyl-2-methylsulfanyl-2-(toluene-4-sulfonyl)-ethyl]-tetrahydro-furan (121669-63-4,121703-45-5,121703-50-2,121703-51-3)

Guidance literature:

With benzophenone; for 1h; Yields of byproduct given; Irradiation;

DOI:10.1016/S0040-4039(00)82875-0

Reference yield: 62.0%

5-hydroxy-1,1-diphenylpentene (1025-23-6) → benzophenone (119-61-9) + 2-(diphenylhydroxymethyl)-tetrahydrofuran (25330-02-3) + 2-(diphenylmethyl)-tetrahydrofuran (86137-41-9)

Guidance literature:

With 9,10-Dicyanoanthracene; oxygen; In acetonitrile; Irradiation;

DOI:10.1016/S0040-4039(00)81437-9

upstream raw materials:

ethyl tetrahydrofurancarboxylate

tetrahydrofuran

1-Methyl-4-((E)-1-methylsulfanyl-prop-1-ene-1-sulfonyl)-benzene

5-hydroxy-1,1-diphenylpentene

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