Benzenamine, 2-nitro-4-[(4-phenyl-1-piperazinyl)methyl]-

Base Information

Chemical Name:Benzenamine, 2-nitro-4-[(4-phenyl-1-piperazinyl)methyl]-
CAS No.:394203-83-9
Molecular Formula:C17H20N4O2
Molecular Weight:312.371
Hs Code.:

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Chemical Property of Benzenamine, 2-nitro-4-[(4-phenyl-1-piperazinyl)methyl]-

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Technology Process of Benzenamine, 2-nitro-4-[(4-phenyl-1-piperazinyl)methyl]-

There total 6 articles about Benzenamine, 2-nitro-4-[(4-phenyl-1-piperazinyl)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 394203-82-8
N-[4-(4-phenylpiperazinyl-1-methyl)-2-nitrophenyl]acetamide

: 394203-83-9
2-nitro-4-(4-phenylpiperazin-1-yl-methyl)phenylamine

Guidance literature:: With hydrogenchloride; for 4h; Heating;

Reference yield:

: 92-54-6
4-phenyl-1-piperazine

: 394203-83-9
2-nitro-4-(4-phenylpiperazin-1-yl-methyl)phenylamine

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / Na₂CO₃; KI / dimethylformamide / 24 h / 80 °C

2: hydrazine hydrate / Raney-Ni / ethanol; 1,2-dichloro-ethane / 50 °C

3: pyridine / CH₂Cl₂ / 24 h / 20 °C

4: 80 percent / HNO₃; conc. H₂SO₄ / acetic anhydride / -5 - 20 °C

5: 90 percent / conc. HCl / 4 h / Heating

With pyridine; hydrogenchloride; sulfuric acid; nitric acid; sodium carbonate; hydrazine hydrate; potassium iodide; nickel; In ethanol; dichloromethane; acetic anhydride; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 40224-22-4
4-(4-phenyl-piperazinyl-methyl)-nitrobenzene

: 394203-83-9
2-nitro-4-(4-phenylpiperazin-1-yl-methyl)phenylamine

Guidance literature:: Multi-step reaction with 4 steps

1: hydrazine hydrate / Raney-Ni / ethanol; 1,2-dichloro-ethane / 50 °C

2: pyridine / CH₂Cl₂ / 24 h / 20 °C

3: 80 percent / HNO₃; conc. H₂SO₄ / acetic anhydride / -5 - 20 °C

4: 90 percent / conc. HCl / 4 h / Heating

With pyridine; hydrogenchloride; sulfuric acid; nitric acid; hydrazine hydrate; nickel; In ethanol; dichloromethane; acetic anhydride; 1,2-dichloro-ethane;