Butanedioic acid, mono[3-[[4-[2-[(3,4-dimethoxyphenyl)methoxy]ethyl]phenyl]methoxy]-2-[[[ 4-[2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]ethyl]phenyl]methoxy]methyl]-2- [[[4-[2-[(tetrahydro-2H-pyran-2-yl)oxy]ethyl]phenyl]methoxy]methyl]propyl] ester

Base Information

Chemical Name:Butanedioic acid, mono[3-[[4-[2-[(3,4-dimethoxyphenyl)methoxy]ethyl]phenyl]methoxy]-2-[[[ 4-[2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]ethyl]phenyl]methoxy]methyl]-2- [[[4-[2-[(tetrahydro-2H-pyran-2-yl)oxy]ethyl]phenyl]methoxy]methyl]propyl] ester
CAS No.:395069-63-3
Molecular Formula:C66H82O13Si
Molecular Weight:1111.45
Hs Code.:

Butanedioic acid,
mono[3-[[4-[2-[(3,4-dimethoxyphenyl)methoxy]ethyl]phenyl]methoxy]-2-[[[
4-[2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]ethyl]phenyl]methoxy]methyl]-2-
[[[4-[2-[(tetrahydro-2H-pyran-2-yl)oxy]ethyl]phenyl]methoxy]methyl]propyl]
ester

Synonyms:

Suppliers and Price of Butanedioic acid, mono[3-[[4-[2-[(3,4-dimethoxyphenyl)methoxy]ethyl]phenyl]methoxy]-2-[[[ 4-[2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]ethyl]phenyl]methoxy]methyl]-2- [[[4-[2-[(tetrahydro-2H-pyran-2-yl)oxy]ethyl]phenyl]methoxy]methyl]propyl] ester

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Chemical Property of Butanedioic acid, mono[3-[[4-[2-[(3,4-dimethoxyphenyl)methoxy]ethyl]phenyl]methoxy]-2-[[[ 4-[2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]ethyl]phenyl]methoxy]methyl]-2- [[[4-[2-[(tetrahydro-2H-pyran-2-yl)oxy]ethyl]phenyl]methoxy]methyl]propyl] ester

Chemical Property:

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Safty Information:

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Technology Process of Butanedioic acid, mono[3-[[4-[2-[(3,4-dimethoxyphenyl)methoxy]ethyl]phenyl]methoxy]-2-[[[ 4-[2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]ethyl]phenyl]methoxy]methyl]-2- [[[4-[2-[(tetrahydro-2H-pyran-2-yl)oxy]ethyl]phenyl]methoxy]methyl]propyl] ester

There total 12 articles about Butanedioic acid, mono[3-[[4-[2-[(3,4-dimethoxyphenyl)methoxy]ethyl]phenyl]methoxy]-2-[[[ 4-[2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]ethyl]phenyl]methoxy]methyl]-2- [[[4-[2-[(tetrahydro-2H-pyran-2-yl)oxy]ethyl]phenyl]methoxy]methyl]propyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 108-30-5
succinic acid anhydride

: 395069-62-2
3-{4-[2-((tert-butyl)diphenylsilyloxy)ethyl]benzyloxy}-2-{4-[2-(3,4-dimethoxybenzyloxy)ethyl]benzyloxymethyl}-2-{4-[2-(tetrahydro-2H-pyran-2-yloxy)ethyl]benzyloxymethyl}propan-1-ol

: 395069-63-3
succinic acid mono-(3-{4-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-benzyloxy}-2-{4-[2-(3,4-dimethoxy-benzyloxy)-ethyl]-benzyloxymethyl}-2-{4-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-benzyloxymethyl}-propyl) ester

Guidance literature:: With dmap; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1021/ol016980p DOI:10.1002/ejoc.200600145

Reference yield:

: 13737-36-5
4-bromophenylacetic acid

: 395069-63-3
succinic acid mono-(3-{4-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-benzyloxy}-2-{4-[2-(3,4-dimethoxy-benzyloxy)-ethyl]-benzyloxymethyl}-2-{4-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-benzyloxymethyl}-propyl) ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: 86 percent / borane-dimethyl sulfide complex / tetrahydrofuran / 4 h / 0 - 20 °C

2.1: 69 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 20 °C

3.1: NaH / tetrahydrofuran / 0.5 h / 40 °C

3.2: 37 percent / tetrabutylammonium iodide / tetrahydrofuran / Heating

4.1: NaH / tetrahydrofuran / 0.5 h / 40 °C

4.2: 32 percent / tetrabutylammonium iodide / tetrahydrofuran / Heating

5.1: 90 percent / DMAP / CH₂Cl₂ / 4 h / 20 °C

With dmap; dimethylsulfide borane complex; pyridinium p-toluenesulfonate; sodium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.200600145

Reference yield:

: 96044-43-8
4-(2-hydroxyethyl)benzyl bromide

: 395069-63-3
succinic acid mono-(3-{4-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-benzyloxy}-2-{4-[2-(3,4-dimethoxy-benzyloxy)-ethyl]-benzyloxymethyl}-2-{4-[2-(tetrahydro-pyran-2-yloxy)-ethyl]-benzyloxymethyl}-propyl) ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: 69 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 20 °C

2.1: NaH / tetrahydrofuran / 0.5 h / 40 °C

2.2: 37 percent / tetrabutylammonium iodide / tetrahydrofuran / Heating

3.1: NaH / tetrahydrofuran / 0.5 h / 40 °C

3.2: 32 percent / tetrabutylammonium iodide / tetrahydrofuran / Heating

4.1: 90 percent / DMAP / CH₂Cl₂ / 4 h / 20 °C

With dmap; pyridinium p-toluenesulfonate; sodium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.200600145