[3-CHLORO-3-(4-METHOXYPHENYL)PROP-2-ENYLIDENE](DIMETHYL)AMMONIUM PERCHLORATE

Base Information

Chemical Name:[3-CHLORO-3-(4-METHOXYPHENYL)PROP-2-ENYLIDENE](DIMETHYL)AMMONIUM PERCHLORATE
CAS No.:39812-29-8
Molecular Formula:C12H15ClNO.ClO4
Molecular Weight:324.16
Hs Code.:
Mol file:39812-29-8.mol

Synonyms:3-Chlor-3-(4-methoxy-phenyl)-N,N-dimethyl-prop-2-enylimmonium;[3-chloro-3-(4-methoxy-phenyl)-allylidene]-dimethyl-ammonium, perchlorate;(γ-Chloro-p-methoxycinnamylidene)dimethylammonium Perchlorate;[3-CHLORO-3-(4-METHOXYPHENYL)PROP-2-ENYLIDENE](DIMETHYL)AMMONIUM PERCHLORATE;

Suppliers and Price of [3-CHLORO-3-(4-METHOXYPHENYL)PROP-2-ENYLIDENE](DIMETHYL)AMMONIUM PERCHLORATE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
(GAMMA-CHLORO-4-METHOXYCINNAMYLIDENE)DIMETHYLAMMONIUM PERCHLORATE Aldrich
250mg
$ 57.00

American Custom Chemicals Corporation
[3-CHLORO-3-(4-METHOXYPHENYL)PROP-2-ENYLIDENE](DIMETHYL)AMMONIUM PERCHLORATE 95.00%
250MG
$ 727.65

Total 4 raw suppliers

Chemical Property of [3-CHLORO-3-(4-METHOXYPHENYL)PROP-2-ENYLIDENE](DIMETHYL)AMMONIUM PERCHLORATE

Chemical Property:

PSA：86.51000
LogP:2.83210

Purity/Quality:

99% ^*data from raw suppliers

(GAMMA-CHLORO-4-METHOXYCINNAMYLIDENE)DIMETHYLAMMONIUM PERCHLORATE Aldrich ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of [3-CHLORO-3-(4-METHOXYPHENYL)PROP-2-ENYLIDENE](DIMETHYL)AMMONIUM PERCHLORATE

There total 4 articles about [3-CHLORO-3-(4-METHOXYPHENYL)PROP-2-ENYLIDENE](DIMETHYL)AMMONIUM PERCHLORATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18096-70-3
3-(dimethylamino)-1-(4-methoxyphenyl)prop-2-en-1-one

: 39812-29-8
<3-chloro-3-(4-methoxyphenyl)-2-propen-1-yliden> dimethyliminium perchlorate

Guidance literature:: With sodium perchlorate; trichlorophosphate; Yield given. Multistep reaction; 1.) anhydr. Dichloromethane, room temp., 20 min; 0 deg C, 10 min, 2.) Dichloromethane/water, 0 deg C, 20 min;
DOI:10.1021/jo01312a011

Reference yield:

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 39812-29-8
<3-chloro-3-(4-methoxyphenyl)-2-propen-1-yliden> dimethyliminium perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / 20 h / Heating

2: 1.) Phosphorus oxychloride, 2.) Sodium perchlorate monohydrate / 1.) anhydr. Dichloromethane, room temp., 20 min; 0 deg C, 10 min, 2.) Dichloromethane/water, 0 deg C, 20 min

With sodium perchlorate; trichlorophosphate;
DOI:10.1021/jo01312a011