2-Amino-6-chlorobenzoic acid methyl ester

Base Information

• Chemical Name: 2-Amino-6-chlorobenzoic acid methyl ester
• CAS No.: 41632-04-6
• Molecular Formula: C8H8ClNO2
• Molecular Weight: 185.61
• Hs Code.: 2922498590
• Mol file: 41632-04-6.mol

Synonyms:2-Amino-6-chlorobenzoic acid methyl ester;6-Chlor-anthranilsaeuremethylester;2-Amino-6-chlor-benzoesaeure-methylester;6-chloro-2-aminobenzoic acid methyl ester;methyl 6-chloro-anthranilate;

Chemical Property of 2-Amino-6-chlorobenzoic acid methyl ester

Chemical Property:

• Boiling Point: 290.4±20.0 °C(Predicted)
• PKA: 1.14±0.10(Predicted)
• PSA: 52.32000
• Density: 1.311±0.06 g/cm3(Predicted)
• LogP: 2.29000

Purity/Quality:

99%, ^*data from raw suppliers

Methyl2-amino-6-chlorobenzoate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Amino-6-chlorobenzoic acid methyl ester

There total 21 articles about 2-Amino-6-chlorobenzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2-chloro-6-aminobenzoic acid (2148-56-3) + methyl iodide (74-88-4) → methyl 6-chloroanthranilate (41632-04-6)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield: 91.0%

2-chloro-6-aminobenzoic acid (2148-56-3) + diazomethyl-trimethyl-silane (18107-18-1) → methyl 6-chloroanthranilate (41632-04-6)

Guidance literature:

In methanol; hexane; benzene; at 20 ℃; for 1h;

Reference yield: 86.0%

2-chloro-6-aminobenzoic acid (2148-56-3) + dimethyl sulfate (77-78-1) → methyl 6-chloroanthranilate (41632-04-6)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

DOI:10.1021/jacs.5b00033

upstream raw materials:

methanol

5-chloro-1H-benzo[d][1,3]oxazine-2,4-dione

diazomethane

2-chloro-6-aminobenzoic acid

Downstream raw materials:

2-(2-Carboxy-phenylamino)-6-chloro-benzoic acid methyl ester

2-Chloro-6-isobutyrylamino-benzoic acid methyl ester

methyl 6-chloro-2-(N-p-toluenesulfonyl)aminobenzoate

2-(2-Carboxy-phenylamino)-6-chloro-benzoic acid

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