3,3-Diphenylacryloyl chloride

Base Information

Chemical Name:3,3-Diphenylacryloyl chloride
CAS No.:4456-79-5
Molecular Formula:C15H11ClO
Molecular Weight:242.705
Hs Code.:
DSSTox Substance ID:DTXSID00460221
Nikkaji Number:J2.315.779I

Synonyms:3,3-diphenylacryloyl chloride;4456-79-5;3,3-diphenyl-acryloyl chloride;SCHEMBL4398750;DTXSID00460221;GAVZPHQMAKWSMG-UHFFFAOYSA-N;1-chloro-3,3-diphenyl-2-propen-1-one

Suppliers and Price of 3,3-Diphenylacryloyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3,3-Diphenylacryloyl chloride

Chemical Property:

XLogP3:4.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:242.0498427
Heavy Atom Count:17
Complexity:263

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=CC(=O)Cl)C2=CC=CC=C2

Technology Process of 3,3-Diphenylacryloyl chloride

There total 9 articles about 3,3-Diphenylacryloyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 606-84-8
3,3-diphenylacrylic acid

: 4456-79-5
3,3-diphenylacryloyl chloride

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide;
DOI:10.1021/jo00798a044

Reference yield:

: 17792-17-5
ethyl 3,3-diphenylacrylate

: 4456-79-5
3,3-diphenylacryloyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 3M methanolic KOH / 1 h / Heating

2: (COCl₂)2 / toluene / 3 h / Heating

With potassium hydroxide; (COCl₂)2; In toluene;
DOI:10.1016/0040-4020(96)00581-9

Reference yield:

: 119-61-9
benzophenone

: 4456-79-5
3,3-diphenylacryloyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / Cooling with ice

1.2: 20 °C

2.1: sodium hydroxide / Reflux

3.1: thionyl chloride / chloroform / 12 h / 20 °C

With thionyl chloride; sodium hydride; sodium hydroxide; In tetrahydrofuran; chloroform; mineral oil;
DOI:10.3998/ark.5550190.0012.230