1-Methyl-4-(1-methyl-ethnenylsulphonyl)benzene

Base Information

Chemical Name:1-Methyl-4-(1-methyl-ethnenylsulphonyl)benzene
CAS No.:67605-02-1
Molecular Formula:C10H12O2S
Molecular Weight:196.27
Hs Code.:
NSC Number:251029
DSSTox Substance ID:DTXSID50217924
Nikkaji Number:J754.132E
Wikidata:Q83094631

Synonyms:1-Methyl-4-(1-methyl-ethnenylsulphonyl)benzene;67605-02-1;NSC251029;SCHEMBL9962546;DTXSID50217924;NSC 251029;NSC-251029;1-METHYL-4-[(1-METHYLETHENYL)SULFONYL]BENZENE

Suppliers and Price of 1-Methyl-4-(1-methyl-ethnenylsulphonyl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1-Methyl-4-(1-methyl-ethnenylsulphonyl)benzene

Chemical Property:

Vapor Pressure:0.000226mmHg at 25°C
Boiling Point:335.9°C at 760 mmHg
Flash Point:186.9°C
Density:1.119g/cm³
XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:196.05580079
Heavy Atom Count:13
Complexity:277

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)C(=C)C

Technology Process of 1-Methyl-4-(1-methyl-ethnenylsulphonyl)benzene

There total 8 articles about 1-Methyl-4-(1-methyl-ethnenylsulphonyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 109898-15-9
3-Acetoxy-2-methyl-2-(toluene-4-sulfonyl)-propionic acid allyl ester

: 67605-02-1
1-Methylethenyl 4-methylphenyl sulfone

Guidance literature:: With triphenylphosphine; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; In acetonitrile; at 25 ℃; for 0.25h;
DOI:10.1246/cl.1987.23

Reference yield: 85.0%

: 536-57-2
p-toluene sulfinic acid

: 74-99-7
prop-1-yne

: 67605-02-1
1-Methylethenyl 4-methylphenyl sulfone

Guidance literature:: With gallium(III) triflate; trimethylpropylsilane; (2-(dicyclohexylphosphino)-3,6-dimethoxy-2',4',6'-triisopropyl-1,1'-biphenyl)Au(1H-benzotriazole)OTf; In 1,2-dichloro-ethane; at 45 ℃; for 24h; Inert atmosphere;
DOI:10.1002/anie.201310142

Reference yield:

: 4964-06-1,4964-07-2,17680-03-4
(E)-prop-1-enyl(trimethyl)stannane

: 824-79-3
sodium 4-methylbenzenesulfinate

: 640-57-3
phenyltolylsulfone

: 32228-15-2
(E)-p-tolyl-1-propenyl sulfone

: 67605-02-1
1-Methylethenyl 4-methylphenyl sulfone

: 66623-35-6
1,2-Bis(4-methylphenylsulfonyl)propane

Guidance literature:: With boron trifluoride diethyl etherate; water; triphenylbismuth(V) difluoride; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₂Cl₂, r.t., 12 h, 2.) DMF, r.t., 12 h;
DOI:10.1039/p19960001971