1H-Indol-4-ol, 5-methoxy-

Base Information

• Chemical Name: 1H-Indol-4-ol, 5-methoxy-
• CAS No.: 49635-16-7
• Molecular Formula: C9H9NO2
• Molecular Weight: 163.17300
• Hs Code.: 2933998090
• Mol file: 49635-16-7.mol

Synonyms:1H-Indazole,5-methoxy;5-methoxy-1(2)H-indazole;5-Methoxy (1H)indazole;5-methoxy-indol-4-ol;5-Methoxyindazole;5-Methoxyindazol;ACMC-209rry;5-Methoxy-1(2)H-indazol;4-Hydroxy-5-methoxy-indole;

Chemical Property of 1H-Indol-4-ol, 5-methoxy-

Chemical Property:

• Melting Point: 152-154 °C(Solv: dichloromethane (75-09-2); hexane (110-54-3))
• Boiling Point: 359.9±22.0 °C(Predicted)
• PKA: 8.22±0.50(Predicted)
• PSA: 45.25000
• Density: 1.312±0.06 g/cm3(Predicted)
• LogP: 1.88210
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

97% ^*data from raw suppliers

5-Methoxy-1H-indol-4-ol 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-Indol-4-ol, 5-methoxy-

There total 9 articles about 1H-Indol-4-ol, 5-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-Benzyloxy-5-methoxyindole (2450-25-1) → 5-methoxy-1H-indol-4-ol (49635-16-7)

Guidance literature:

In 4-benzyloxy-5-ethoxyindole;

Reference yield: 58.0%

2-(benzyloxy)-1-methoxy-4-nitro-3-(2-nitrovinyl)benzene (2426-62-2) → 5-methoxy-1H-indol-4-ol (49635-16-7)

Guidance literature:

With 10% palladium on carbon; hydrogen; acetic acid; In ethanol; at 20 ℃; for 8h; under 750.075 Torr;

DOI:10.1016/j.ejmech.2009.07.012

Reference yield: 54.0%

4-acetoxy-5-methoxyindole (213040-72-3) → 5-methoxy-1H-indol-4-ol (49635-16-7)

Guidance literature:

With sodium hydroxide; sodium dithionite; In N,N-dimethyl-formamide; at 5 ℃; for 0.333333h;

DOI:10.1016/S0040-4020(98)00593-6

upstream raw materials:

4-acetoxy-5-methoxyindole

2-hydroxy-3-methoxy-6-nitrobenzaldehyde

5,6-dimethoxy-2-nitrobenzaldehyde

2-acetoxy-3-methoxy-6-nitro-benzaldehyde

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