2,3-DIMETHOXY-6-NITRO-BENZALDEHYDE

Base Information

• Chemical Name: 2,3-DIMETHOXY-6-NITRO-BENZALDEHYDE
• CAS No.: 2531-63-7
• Molecular Formula: C9H9NO5
• Molecular Weight: 211.174
• Hs Code.: 2913000090
• Mol file: 2531-63-7.mol

Synonyms:5,6-dimethoxy-2-nitrobenzaldehyde;2,3-Dimethoxy-6-nitro-benzaldehyd;2,3-Dimethoxy-6-nitrobenzaldehyde;2,3-dimethoxy-6-nitro-benzaldehyde;

Chemical Property of 2,3-DIMETHOXY-6-NITRO-BENZALDEHYDE

Chemical Property:

• PSA: 81.35000
• LogP: 1.94770

Purity/Quality:

99% ^*data from raw suppliers

2,3-Dimethoxy-6-nitrobenzaldehyde 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,3-DIMETHOXY-6-NITRO-BENZALDEHYDE

There total 18 articles about 2,3-DIMETHOXY-6-NITRO-BENZALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

2-Hydroxy-3-methoxy-6-nitrobenzaldehyde, sodium salt (111042-36-5) + dimethyl sulfate (77-78-1) → 5,6-dimethoxy-2-nitrobenzaldehyde (2531-63-7)

Guidance literature:

With potassium carbonate; In acetone; for 84h; Heating;

DOI:10.1002/jhet.5570230643

Reference yield: 46.0%

2,3-dimethyoxybenzaldehyde (86-51-1) → 5,6-dimethoxy-2-nitrobenzaldehyde (2531-63-7) + 2,3-dimethoxy-5-nitrobenzaldehyde (6324-49-8)

Guidance literature:

With nitric acid; In acetic acid; for 0.75h; Ambient temperature;

DOI:10.1016/S0040-4020(98)00593-6

Reference yield:

2-Hydroxy-3-methoxy-6-nitrobenzaldehyde potassium salt (103483-19-8) → 5,6-dimethoxy-2-nitrobenzaldehyde (2531-63-7)

Guidance literature:

With potassium carbonate; dimethyl sulfate; In water;

upstream raw materials:

2-hydroxy-3-methoxy-6-nitrobenzaldehyde

dimethyl sulfate

2,3-dimethyoxybenzaldehyde

methyl iodide

Downstream raw materials:

2,3-dimethoxy-6-nitrobenzoic acid

6-amino-2,3-dimethoxy-benzaldehyde

2,3-dimethoxy-6-nitro-benzyl alcohol

2,3-dimethoxy-6-nitro-benzaldehyde-oxime

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