2-Oxa-4,8,13-triazatetradecan-14-oic acid, 8-[(2S)-2-[[[(2S,3S)-3-(ethoxycarbonyl)oxiranyl]carbonyl]amino]-1-oxo-3 -[4-(phenylmethoxy)phenyl]propyl]-3-oxo-1-phenyl-, phenylmethyl ester

Base Information

Chemical Name:2-Oxa-4,8,13-triazatetradecan-14-oic acid, 8-[(2S)-2-[[[(2S,3S)-3-(ethoxycarbonyl)oxiranyl]carbonyl]amino]-1-oxo-3 -[4-(phenylmethoxy)phenyl]propyl]-3-oxo-1-phenyl-, phenylmethyl ester
CAS No.:500228-05-7
Molecular Formula:C45H52N4O10
Molecular Weight:808.929
Hs Code.:

2-Oxa-4,8,13-triazatetradecan-14-oic acid,
8-[(2S)-2-[[[(2S,3S)-3-(ethoxycarbonyl)oxiranyl]carbonyl]amino]-1-oxo-3
-[4-(phenylmethoxy)phenyl]propyl]-3-oxo-1-phenyl-, phenylmethyl ester

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Chemical Property of 2-Oxa-4,8,13-triazatetradecan-14-oic acid, 8-[(2S)-2-[[[(2S,3S)-3-(ethoxycarbonyl)oxiranyl]carbonyl]amino]-1-oxo-3 -[4-(phenylmethoxy)phenyl]propyl]-3-oxo-1-phenyl-, phenylmethyl ester

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Technology Process of 2-Oxa-4,8,13-triazatetradecan-14-oic acid, 8-[(2S)-2-[[[(2S,3S)-3-(ethoxycarbonyl)oxiranyl]carbonyl]amino]-1-oxo-3 -[4-(phenylmethoxy)phenyl]propyl]-3-oxo-1-phenyl-, phenylmethyl ester

There total 5 articles about 2-Oxa-4,8,13-triazatetradecan-14-oic acid, 8-[(2S)-2-[[[(2S,3S)-3-(ethoxycarbonyl)oxiranyl]carbonyl]amino]-1-oxo-3 -[4-(phenylmethoxy)phenyl]propyl]-3-oxo-1-phenyl-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 63734-73-6,66647-16-3,68521-71-1,89886-73-7,93061-20-2,149884-11-7
ethyl (2S,3S)-2,3-epoxysuccinate

: 500228-04-6
(+)-{{4-{(2S)-2-Amino-3-[4-(benzyloxy)phenyl]propanoyl}{3-{[(benzyloxy)carbonyl]amino}propyl}amino}butyl}carbonsaeure-benzylester

: 500228-05-7
(+)-(2S,3S)-3-{{(1S)-1-{{4-{[(Benzyloxy)carbonyl]amino}butyl}{3-{[(benzyloxy)carbonyl]amino}propyl}carbamoyl}-2'-[4-(benzyloxy)phenyl]ethyl}carbamoyl}oxiran-2-carbonsaeure-ethylester

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In ethyl acetate; at 20 ℃; for 2h;
DOI:10.1002/hlca.200390015

Reference yield:

: 2130-96-3,54784-43-9
O-benzyl-N-tert-butoxycarbonyl-L-tyrosine

: 500228-05-7
(+)-(2S,3S)-3-{{(1S)-1-{{4-{[(Benzyloxy)carbonyl]amino}butyl}{3-{[(benzyloxy)carbonyl]amino}propyl}carbamoyl}-2'-[4-(benzyloxy)phenyl]ethyl}carbamoyl}oxiran-2-carbonsaeure-ethylester

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / HOBT; DCC / CH₂Cl₂; ethyl acetate / 2 h / 20 °C

2: 100 percent / trifluoroacetic acid / toluene / 1 h / 20 °C

3: 88 percent / HOBT; DCC / ethyl acetate / 2 h / 20 °C

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; ethyl acetate; toluene;
DOI:10.1002/hlca.200390015

Reference yield:

: 89965-56-0
<3-<<4-(carboxyamino)butyl>amino>propyl>carbamic acid, dibenzyl ester

: 500228-05-7
(+)-(2S,3S)-3-{{(1S)-1-{{4-{[(Benzyloxy)carbonyl]amino}butyl}{3-{[(benzyloxy)carbonyl]amino}propyl}carbamoyl}-2'-[4-(benzyloxy)phenyl]ethyl}carbamoyl}oxiran-2-carbonsaeure-ethylester

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / HOBT; DCC / CH₂Cl₂; ethyl acetate / 2 h / 20 °C

2: 100 percent / trifluoroacetic acid / toluene / 1 h / 20 °C

3: 88 percent / HOBT; DCC / ethyl acetate / 2 h / 20 °C

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; ethyl acetate; toluene;
DOI:10.1002/hlca.200390015