(+)-{{4-{(2S)-2-Amino-3-[4-(benzyloxy)phenyl]propanoyl}{3-{[(benzyloxy)carbonyl]amino}propyl}amino}butyl}carbonsaeure-benzylester

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Chemical Name:(+)-{{4-{(2S)-2-Amino-3-[4-(benzyloxy)phenyl]propanoyl}{3-{[(benzyloxy)carbonyl]amino}propyl}amino}butyl}carbonsaeure-benzylester
CAS No.:500228-04-6
Molecular Formula:C₃₉H₄₆N₄O₆
Molecular Weight:666.817
Hs Code.:

Synonyms:(+)-{{4-{(2S)-2-Amino-3-[4-(benzyloxy)phenyl]propanoyl}{3-{[(benzyloxy)carbonyl]amino}propyl}amino}butyl}carbonsaeure-benzylester

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Chemical Property of (+)-{{4-{(2S)-2-Amino-3-[4-(benzyloxy)phenyl]propanoyl}{3-{[(benzyloxy)carbonyl]amino}propyl}amino}butyl}carbonsaeure-benzylester

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Technology Process of (+)-{{4-{(2S)-2-Amino-3-[4-(benzyloxy)phenyl]propanoyl}{3-{[(benzyloxy)carbonyl]amino}propyl}amino}butyl}carbonsaeure-benzylester

There total 3 articles about (+)-{{4-{(2S)-2-Amino-3-[4-(benzyloxy)phenyl]propanoyl}{3-{[(benzyloxy)carbonyl]amino}propyl}amino}butyl}carbonsaeure-benzylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 500228-03-5
(+)-{4-{{3-{[(Benzyloxy)carbonyl]amino}propyl}{(2S)-3-[(4-benzyloxy)phenyl]-2-{[(tert-butoxy)carbonyl]amino}propanoyl}amino}butyl}carbaminsaeure-benzylester

: 500228-04-6
(+)-{{4-{(2S)-2-Amino-3-[4-(benzyloxy)phenyl]propanoyl}{3-{[(benzyloxy)carbonyl]amino}propyl}amino}butyl}carbonsaeure-benzylester

Guidance literature:: With trifluoroacetic acid; In toluene; at 20 ℃; for 1h;
DOI:10.1002/hlca.200390015

Reference yield:

: 2130-96-3,54784-43-9
O-benzyl-N-tert-butoxycarbonyl-L-tyrosine

: 500228-04-6
(+)-{{4-{(2S)-2-Amino-3-[4-(benzyloxy)phenyl]propanoyl}{3-{[(benzyloxy)carbonyl]amino}propyl}amino}butyl}carbonsaeure-benzylester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / HOBT; DCC / CH₂Cl₂; ethyl acetate / 2 h / 20 °C

2: 100 percent / trifluoroacetic acid / toluene / 1 h / 20 °C

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; ethyl acetate; toluene;
DOI:10.1002/hlca.200390015

Reference yield:

: 89965-56-0
<3-<<4-(carboxyamino)butyl>amino>propyl>carbamic acid, dibenzyl ester

: 500228-04-6
(+)-{{4-{(2S)-2-Amino-3-[4-(benzyloxy)phenyl]propanoyl}{3-{[(benzyloxy)carbonyl]amino}propyl}amino}butyl}carbonsaeure-benzylester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / HOBT; DCC / CH₂Cl₂; ethyl acetate / 2 h / 20 °C

2: 100 percent / trifluoroacetic acid / toluene / 1 h / 20 °C

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; ethyl acetate; toluene;
DOI:10.1002/hlca.200390015