2-Amino-3,6-dimethoxybenzoic acid

Base Information

Chemical Name:2-Amino-3,6-dimethoxybenzoic acid
CAS No.:50472-10-1
Molecular Formula:C9H11NO4
Molecular Weight:197.191
Hs Code.:2922509090
European Community (EC) Number:877-524-9
DSSTox Substance ID:DTXSID40360973
Nikkaji Number:J89.556C
Wikidata:Q82143029
Mol file:50472-10-1.mol

Synonyms:2-amino-3,6-dimethoxybenzoic acid;50472-10-1;2-amino-3,6-dimethoxybenzoicacid;Oprea1_867105;AG-777/36176021;SCHEMBL6382450;DTXSID40360973;RRQMXQWSIJERLR-UHFFFAOYSA-N;CS-0237960;EN300-188452;Z594219062

Suppliers and Price of 2-Amino-3,6-dimethoxybenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
2-Amino-3,6-dimethoxybenzoicacid 97%
10g
$ 4500.00

Matrix Scientific
2-Amino-3,6-dimethoxybenzoicacid 97%
5g
$ 2880.00

Crysdot
2-Amino-3,6-dimethoxybenzoicacid 95+%
5g
$ 2857.00

American Custom Chemicals Corporation
2-AMINO-3,6-DIMETHOXYBENZOIC ACID 95.00%
5MG
$ 501.56

AK Scientific
2-Amino-3,6-dimethoxybenzoicacid
250mg
$ 370.00

Total 2 raw suppliers

Chemical Property of 2-Amino-3,6-dimethoxybenzoic acid

Chemical Property:

PSA：81.78000
LogP:1.56540
XLogP3:0.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:197.06880783
Heavy Atom Count:14
Complexity:209

Purity/Quality:

99% ^*data from raw suppliers

2-Amino-3,6-dimethoxybenzoicacid 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C(=C(C=C1)OC)N)C(=O)O

Technology Process of 2-Amino-3,6-dimethoxybenzoic acid

There total 5 articles about 2-Amino-3,6-dimethoxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 50472-09-8
3,6-dimethoxy-2-nitrobenzoic acid

: 50472-10-1
2-amino-3,6-dimethoxybenzoic acid

Guidance literature:: With ammonium formate; palladium on activated charcoal; In ethanol; at 70 ℃; for 7h;
DOI:10.1016/S0040-4020(98)00797-2

Reference yield:

: 2785-98-0
2,5-dimethoxybenzoic acid

: 50472-10-1
2-amino-3,6-dimethoxybenzoic acid

Guidance literature:: With hydrogen; nitric acid; palladium on activated charcoal; Yield given. Multistep reaction; 1.) from 0 deg C to 5 deg C, 3 h, 2.) ethyl acetate;
DOI:10.1246/bcsj.56.302

Reference yield:

: 93-02-7
2,5-dimethoxybenzaldehyde

: 50472-10-1
2-amino-3,6-dimethoxybenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / potassium permanganate / H₂O / 1 h / 80 °C

2: 72 percent / cc. nitric acid / 3 h / 0 - 2 °C

3: 93 percent / H₂ / 10 percent Pd-C / ethanol / 6 h / 38000 Torr

With potassium permanganate; hydrogen; nitric acid; palladium on activated charcoal; In ethanol; water;
DOI:10.1016/S0040-4020(01)81452-6