Methyl 2-(benzyloxy)-5-nitrobenzenecarboxylate

Base Information

• Chemical Name: Methyl 2-(benzyloxy)-5-nitrobenzenecarboxylate
• CAS No.: 508211-52-7
• Molecular Formula: C15H13NO5
• Molecular Weight: 287.272
• Hs Code.: 2918990090
• Mol file: 508211-52-7.mol

Synonyms:Methyl 2-(benzyloxy)-5-nitrobenzoate;2-benzyloxy-5-nitro-benzoic acid methyl ester;HD-0002;Methyl 2-(benzyloxy)-5-nitrobenzenecarboxylate;2-Benzyloxy-5-nitro-benzoesaeure-methylester;

Chemical Property of Methyl 2-(benzyloxy)-5-nitrobenzenecarboxylate

Chemical Property:

• Melting Point: 74-76°
• PSA: 81.35000
• LogP: 3.48360

Purity/Quality:

98%min ^*data from raw suppliers

Methyl 2-(benzyloxy)-5-nitrobenzoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Methyl 2-(benzyloxy)-5-nitrobenzenecarboxylate

There total 2 articles about Methyl 2-(benzyloxy)-5-nitrobenzenecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.2%

methyl 2-hydroxy-5-nitrobenzoate (17302-46-4) + benzyl bromide (100-39-0) → 2-benzyloxy-5-nitro-benzoic acid methyl ester (508211-52-7)

Guidance literature:

In N,N-dimethyl-formamide; at 60 - 80 ℃;

Reference yield:

methanol (67-56-1) + 2-benzyloxy-5-nitrobenzoic acid (874523-84-9) → 2-benzyloxy-5-nitro-benzoic acid methyl ester (508211-52-7)

Guidance literature:

With sulfuric acid;

Reference yield: 86.0%

2-benzyloxy-5-nitro-benzoic acid methyl ester (508211-52-7) → 5-amino-2-benzyloxybenzoic acid methyl ester

Guidance literature:

With sodium tetrahydroborate; nickel(II) chloride hexahydrate; In methanol; at 20 ℃;

upstream raw materials:

methanol

2-benzyloxy-5-nitrobenzoic acid

methyl 2-hydroxy-5-nitrobenzoate

benzyl bromide

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