1H-Indole, 4,5,6,7-tetrahydro-1-methyl-

Base Information

• Chemical Name: 1H-Indole, 4,5,6,7-tetrahydro-1-methyl-
• CAS No.: 51265-33-9
• Molecular Formula: C9H13N
• Molecular Weight: 135.209
• Mol file: 51265-33-9.mol

Synonyms:1-Methyl-2,3-tetramethylenpyrrol;1-Methyl-4,5,6,7-tetrahydroindol;1-methyl-4,5,6,7-tetrahydro-indole;4,5,6,7-tetrahydro-1-methylindole;N-methyl-4,5,6,7-tetrahydroindole;

Chemical Property of 1H-Indole, 4,5,6,7-tetrahydro-1-methyl-

Chemical Property:

• Boiling Point: 93-95 °C(Press: 17.5 Torr)
• PSA: 4.93000
• Density: 0.9967 g/cm3
• LogP: 1.90390

Purity/Quality:

98% ^*data from raw suppliers

4,5,6,7-tetrahydro-1-methyl-1H-Indole 97.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-Indole, 4,5,6,7-tetrahydro-1-methyl-

There total 13 articles about 1H-Indole, 4,5,6,7-tetrahydro-1-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

1-methyl-octahydroindole (1194-58-7,2030-25-3,15248-51-8) → 1-methyl-4,5,6,7-tetrahydro-1H-indole (51265-33-9)

Guidance literature:

With chlorohydrido(2,6-bis(di-tert-butylphosphinito)phen-1-yl)iridium(III); sodium t-butanolate; at 195 ℃; for 48h; Schlenk technique; Inert atmosphere;

DOI:10.1039/c4cc02073a

Reference yield: 72.0%

4-methyl-1-oxa-4-azaspiro<4.5>decane (39931-24-3) → (2-hydroxyethyl)(methyl)amine (109-83-1) + 1-methyl-4,5,6,7-tetrahydro-1H-indole (51265-33-9) + cyclohexanol (108-93-0)

Guidance literature:

With potassium hydroxide; Heating; CH₃ONa sa reagent;

DOI:10.1007/BF00542786

Reference yield:

1-methyl-octahydroindole (1194-58-7,2030-25-3,15248-51-8) → 1-methylindole (603-76-9) + 1-methyl-4,5,6,7-tetrahydro-1H-indole (51265-33-9)

Guidance literature:

silica gel; palladium; at 165 ℃; for 5h;

DOI:10.1039/b718209k

upstream raw materials:

4-methyl-1-oxa-4-azaspiro<4.5>decane

cyclohexanone

methylamine

2-Chloroacrylonitrile

Downstream raw materials:

N-<2,2,2-trichloro-1-(1-methyl-4,5,6,7-tetrahydro-2-indolyl)ethyl>-p-chlorobenzenesulfonamide

1-phenyl-3-(1-methyl-4,5,6,7-tetrahydro-1H-indol-2-yl)-2-propynone

(2Z,2'Z)-3,3'-[ethane-1,2-diylbis(azanediyl)]bis(3-(1-methyl-4,5,6,7-tetrahydro-1H-indol-2-yl)-1-phenylprop-2-en-1-one)

acetophenone

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