Benzene, (1-methyl-1,2-butadienyl)-

Base Information

Chemical Name:Benzene, (1-methyl-1,2-butadienyl)-
CAS No.:52741-30-7
Molecular Formula:C11H12
Molecular Weight:144.216
Hs Code.:
DSSTox Substance ID:DTXSID00441313
Nikkaji Number:J680.805K

Synonyms:52741-30-7;Benzene, (1-methyl-1,2-butadienyl)-;2-Phenyl-2,3-pentadiene;DTXSID00441313

Suppliers and Price of Benzene, (1-methyl-1,2-butadienyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Benzene, (1-methyl-1,2-butadienyl)-

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:144.093900383
Heavy Atom Count:11
Complexity:165

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC=C=C(C)C1=CC=CC=C1

Technology Process of Benzene, (1-methyl-1,2-butadienyl)-

There total 8 articles about Benzene, (1-methyl-1,2-butadienyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 917-64-6
methyl magnesium iodide

: 58202-94-1
2-phenylethynyl-1,3-dithiane

: 52741-30-7
(1-methyl-1,2-butadienyl)benzene

Guidance literature:: With [1,1'-bis(diphenylphosphino)ferrocene]nickel(II) chloride; potassium iodide; In tetrahydrofuran; benzene; at 65 ℃; for 12h;
DOI:10.1021/jo961514c

Reference yield: 83.0%

: 13154-14-8,13154-15-9,14092-04-7,1730-25-2
1-propenylmagnesium bromide

: 98-86-2
acetophenone

: 52741-30-7
(1-methyl-1,2-butadienyl)benzene

Guidance literature:: With bis(cyclopentadienyl)titanium dichloride; Product distribution; multistep reaction: 1.) THF, -40 deg C to 0 deg C, 1.5 h, 2.) room temperature; allylation of carbonyl compounds with alkenyltitanocene derivatives;
DOI:10.1021/jo9620876