Benzenemethanethiol, lithium salt

Base Information

• Chemical Name: Benzenemethanethiol, lithium salt
• CAS No.: 52791-97-6
• Molecular Formula: C7H8S.Li
• Molecular Weight: 130.14

Synonyms:

Chemical Property of Benzenemethanethiol, lithium salt

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

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Technology Process of Benzenemethanethiol, lithium salt

There total 1 articles about Benzenemethanethiol, lithium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

dibenzyl disulphide (150-60-7) + 1-indene (95-13-6) → 3-(thiobenzyl)indene (1250347-12-6) + lithium phenylmethanethiolate (52791-97-6)

Guidance literature:

1-indene; With n-butyllithium; In hexane; for 12h; Inert atmosphere; Cooling with ice;

dibenzyl disulphide; In hexane; at 20 ℃; Inert atmosphere;

DOI:10.1080/00958971003690447

Reference yield: 90.0%

2,5-Dimethyl-6-phenyl-cyclohex-3-enecarboxylic acid ((1S,2R)-2-hydroxy-1-methyl-2-phenyl-ethyl)-amide (130178-09-5) + lithium phenylmethanethiolate (52791-97-6) → 2,5-Dimethyl-6-phenyl-cyclohex-3-enecarbothioic acid S-benzyl ester (130178-11-9)

Guidance literature:

In tetrahydrofuran; at 25 ℃; for 18h;

DOI:10.1016/0040-4039(90)80164-H

Reference yield: 90.0%

lithium phenylmethanethiolate (52791-97-6) + (4S,5R)-3-{(E)-3-[(1S,2R,5S,6S)-6-(4-Fluoro-phenyl)-2,5-dimethyl-cyclohex-3-enyl]-acryloyl}-4-methyl-5-phenyl-oxazolidin-2-one (130272-31-0) → (E)-3-[(1S,2R,5S,6S)-6-(4-Fluoro-phenyl)-2,5-dimethyl-cyclohex-3-enyl]-thioacrylic acid S-benzyl ester (130178-14-2)

Guidance literature:

In tetrahydrofuran; at -25 ℃; for 0.166667h;

DOI:10.1016/0040-4039(90)80164-H

upstream raw materials:

dibenzyl disulphide

1-indene

Downstream raw materials:

2-Benzylthio-3,3-dimethyl-3H-indole

2,5-Dimethyl-6-phenyl-cyclohex-3-enecarbothioic acid S-benzyl ester

(E)-3-[(1S,2R,5S,6S)-6-(4-Fluoro-phenyl)-2,5-dimethyl-cyclohex-3-enyl]-thioacrylic acid S-benzyl ester

2-(2-Benzylsulfanylmethyl-phenylsulfanyl)-tetrahydro-furan

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