1-Methoxy-2-[(E)-2-phenylethenyl]benzene

Base Information

• Chemical Name: 1-Methoxy-2-[(E)-2-phenylethenyl]benzene
• CAS No.: 52805-92-2
• Molecular Formula: C15H14O
• Molecular Weight: 210.276
• Hs Code.: 2909309090
• Mol file: 52805-92-2.mol

Synonyms:1-Methoxy-2-[(E)-2-phenylethenyl]benzene;Benzene, 1-methoxy-2-(2-phenylethenyl)-, (E)-;

Chemical Property of 1-Methoxy-2-[(E)-2-phenylethenyl]benzene

Chemical Property:

• PSA: 9.23000
• LogP: 3.86560

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Methoxy-2-[(E)-2-phenylethenyl]benzene

There total 113 articles about 1-Methoxy-2-[(E)-2-phenylethenyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + 2-bromoanisole (578-57-4) → (E)-2-methoxystilbene (52805-92-2)

Guidance literature:

With (1-adamantyl)di(tert-butyl) phosphine; triethylamine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 20 ℃; for 20h;

DOI:10.1021/ja0058435

Reference yield: 97.0%

iodobenzene (591-50-4) + o-methoxystyrene (612-15-7) → (E)-2-methoxystilbene (52805-92-2)

Guidance literature:

With 1-[2-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyloxy)ethyl]-3-[2-hydroxy-(2,4-dichlorophenyl)ethyl]imidazolium bromide; potassium tert-butylate; potassium carbonate; palladium dichloride; In tetrahydrofuran; water; at 60 - 90 ℃; for 6h; Inert atmosphere; Sealed tube;

DOI:10.1016/j.carres.2020.108079

Reference yield: 97.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + 4-iodoanisol (529-28-2) → (E)-2-methoxystilbene (52805-92-2)

Guidance literature:

With potassium phosphate; C₂₈H₃₃Cl₂N₃Pd; In N,N-dimethyl acetamide; at 110 ℃; for 18h; Reagent/catalyst; Inert atmosphere;

DOI:10.1007/s11243-013-9700-1

upstream raw materials:

1-(2-methoxyphenyl)-2-phenylethanol

(Z)-1-(2-methoxyphenyl)-2-phenylethene

4-iodoanisol

cinnamylacetate

Downstream raw materials:

(E)-2-hydroxystilbene

1-methoxyphenanthrene

1-(naphthalen-2-yl)butan-1-one

C₁₉H₂₂OS₂