2-Ethoxy-N,N-diethylbenzamide

Base Information

Chemical Name:2-Ethoxy-N,N-diethylbenzamide
CAS No.:3688-82-2
Molecular Formula:C₁₃H₁₉NO₂
Molecular Weight:221.299
Hs Code.:2924299090
Mol file:3688-82-2.mol

Synonyms:Benzamide,N,N-diethyl-o-methoxy- (4CI); Benzamide, o-ethoxy-N,N-diethyl- (6CI,7CI,8CI);2-Ethoxy-N,N-diethylbenzamide; ENT 20297; N,N-Diethyl-2-ethoxybenzamide; NSC7152; R 176; o-Ethoxy-N,N-diethylbenzamide

Suppliers and Price of 2-Ethoxy-N,N-diethylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-Ethoxy-N,N-diethylbenzamide

Chemical Property:

Vapor Pressure:2.58E-05mmHg at 25°C
Boiling Point:358.2°Cat760mmHg
PKA:-0.78±0.70(Predicted)
Flash Point:170.5°C
PSA：29.54000
Density:1.013g/cm³
LogP:2.56730

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Ethoxy-N,N-diethylbenzamide

There total 1 articles about 2-Ethoxy-N,N-diethylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42926-52-3
2-ethoxybenzoyl chloride

: 109-89-7
diethylamine

: 3688-82-2
N,N-diethyl-2-ethoxybenzamide

Guidance literature:: DOI:10.1021/jo01369a003

Reference yield:

: 3688-82-2
N,N-diethyl-2-ethoxybenzamide

: 139213-32-4
2-Ethoxy-N,N-diethyl-6-sulfamoyl-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1) s-BuLi, N,N,N',N'-tetramethylethylenediamine, 2) SO₂ / 1) THF, -78 deg C, 90 min, 2) to r.t., 16 h

2: NH₂OSO₃H, NaOH / H₂O / 6 h / Ambient temperature

With sodium hydroxide; N,N,N,N,-tetramethylethylenediamine; sulfur dioxide; sec.-butyllithium; hydroxylamine-O-sulfonic acid; In water;
DOI:10.1016/0040-4039(91)80470-Q