Benzene, 1-(1,1-dimethoxyethyl)-4-methyl-

Base Information

Chemical Name:Benzene, 1-(1,1-dimethoxyethyl)-4-methyl-
CAS No.:53578-01-1
Molecular Formula:C11H16O2
Molecular Weight:180.247
Hs Code.:
DSSTox Substance ID:DTXSID80448365
Nikkaji Number:J609.810J
Wikidata:Q82267333
Mol file:53578-01-1.mol

Synonyms:53578-01-1;Benzene, 1-(1,1-dimethoxyethyl)-4-methyl-;SCHEMBL7609864;DTXSID80448365;p-MethylacetophenoneDimethylAcetal;4'-Methylacetophenone dimethyl acetal

Suppliers and Price of Benzene, 1-(1,1-dimethoxyethyl)-4-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Benzene, 1-(1,1-dimethoxyethyl)-4-methyl-

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:180.115029749
Heavy Atom Count:13
Complexity:144

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C(C)(OC)OC

Technology Process of Benzene, 1-(1,1-dimethoxyethyl)-4-methyl-

There total 14 articles about Benzene, 1-(1,1-dimethoxyethyl)-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.8%

: 67-56-1
methanol

: 122-00-9
para-methylacetophenone

: 149-73-5
trimethyl orthoformate

: 53578-01-1
4-methylacetophenone dimethyl acetal

Guidance literature:: With povidone-iodine; at 30 ℃; for 6h; Green chemistry;
DOI:10.1016/j.tet.2021.132250

Reference yield: 94.0%

: 122-00-9
para-methylacetophenone

: 149-73-5
trimethyl orthoformate

: 53578-01-1
4-methylacetophenone dimethyl acetal

Guidance literature:: With toluene-4-sulfonic acid; In methanol; at 25 ℃; for 18h; Inert atmosphere;
DOI:10.1021/acs.orglett.9b02273

Reference yield:

: 67-56-1
methanol

: 766-97-2
4-n-methylphenylacetylene

: 53578-01-1
4-methylacetophenone dimethyl acetal

: 122-00-9
para-methylacetophenone

Guidance literature:: With Echavarren's catalyst; In dichloromethane; at 20 ℃; for 24h; Time; Temperature; Inert atmosphere; Sealed tube;
DOI:10.1016/j.jfluchem.2017.01.004