1-phenyl-1H-1,3-benzodiazol-5-amine

Base Information

Chemical Name:1-phenyl-1H-1,3-benzodiazol-5-amine
CAS No.:53897-95-3
Molecular Formula:C13H11N3
Molecular Weight:209.25
Hs Code.:
European Community (EC) Number:849-530-1
DSSTox Substance ID:DTXSID90359478
Wikidata:Q82140705
ChEMBL ID:CHEMBL150973
Mol file:53897-95-3.mol

Synonyms:1-phenyl-1H-1,3-benzodiazol-5-amine;53897-95-3;1-phenylbenzimidazol-5-amine;5-Amino-1-phenylbenzimidazole;1-Phenylbenzimidazole deriv. 71;Oprea1_770736;BDBM3854;CHEMBL150973;SCHEMBL2311242;DTXSID90359478;JSQMNGQWESPAOF-UHFFFAOYSA-N;1-phenyl-1H-benzimidazol-5-amine;STL282760;AKOS000268841;EN300-112672;SR-01000490978;SR-01000490978-1;Z57290870

Suppliers and Price of 1-phenyl-1H-1,3-benzodiazol-5-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1-phenyl-1H-1,3-benzodiazol-5-amine

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:209.095297364
Heavy Atom Count:16
Complexity:237

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)N2C=NC3=C2C=CC(=C3)N

Technology Process of 1-phenyl-1H-1,3-benzodiazol-5-amine

There total 11 articles about 1-phenyl-1H-1,3-benzodiazol-5-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 15127-88-5
5-nitro-1-phenyl-1H-benzo[d]imidazole

: 53897-95-3
1-phenylbenzimidazol-5-amine

Guidance literature:: With sodium dithionite; water; In ethanol; for 4h; Reflux;
DOI:10.1021/acs.inorgchem.9b01678

Reference yield: 61.0%

: 64-18-6
formic acid

: 961-68-2
N-phenyl-2,4-dinitroaniline

: 53897-95-3
1-phenylbenzimidazol-5-amine

: 15127-88-5
5-nitro-1-phenyl-1H-benzo[d]imidazole

Guidance literature:: N-phenyl-2,4-dinitroaniline; With hydrogen; palladium 10% on activated carbon; In ethyl acetate; for 52h;

formic acid; With hydrogenchloride; In water; at 78 - 80 ℃; for 22h; Inert atmosphere;

With sodium hydroxide; In water; at 20 ℃; pH=12;

Reference yield:

: 64-18-6
formic acid

: 136-17-4
2,4-diaminodiphenylamine

: 53897-95-3
1-phenylbenzimidazol-5-amine

Guidance literature:: formic acid; 2,4-diaminodiphenylamine; With hydrogenchloride; In water; at 100 ℃; for 1.5h;

With sodium hydroxide; In water; at 20 ℃; pH=~ 13;