Benzenamine, N-methyl-2-[(4-methylphenyl)sulfonyl]-

Base Information

Chemical Name:Benzenamine, N-methyl-2-[(4-methylphenyl)sulfonyl]-
CAS No.:53973-85-6
Molecular Formula:C14H15NO2S
Molecular Weight:261.345
Hs Code.:
DSSTox Substance ID:DTXSID80487799
Wikidata:Q82330039
Mol file:53973-85-6.mol

Synonyms:Benzenamine, N-methyl-2-[(4-methylphenyl)sulfonyl]-;53973-85-6;DTXSID80487799

Suppliers and Price of Benzenamine, N-methyl-2-[(4-methylphenyl)sulfonyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenamine, N-methyl-2-[(4-methylphenyl)sulfonyl]-

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:261.08234989
Heavy Atom Count:18
Complexity:353

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)C2=CC=CC=C2NC

Technology Process of Benzenamine, N-methyl-2-[(4-methylphenyl)sulfonyl]-

There total 6 articles about Benzenamine, N-methyl-2-[(4-methylphenyl)sulfonyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 32857-49-1
N-(4-bromophenyl)-N,4-dimethylbenzenesulfonamide

: 53973-85-6
N-Methyl-2-(4-methylphenylsulfonyl)benzolamin

Guidance literature:: With n-butyllithium; In tetrahydrofuran; -105 degC -> room temp.;

Reference yield: 26.0%

: 599-62-2
N-methyl-N-phenyltoluenesulfonamide

: 53973-85-6
N-Methyl-2-(4-methylphenylsulfonyl)benzolamin

: 100-61-8
N-methylaniline

: 2835-77-0
(2-aminophenyl)(phenyl)methanone

: methyl-[4-(toluene-4-sulfonyl)-phenyl]-amine

Guidance literature:: In acetonitrile; for 4h; Irradiation;
DOI:10.1016/j.tet.2003.08.006

Reference yield:

: 32857-48-0
N-(4-bromophenyl)-4-methylbenzenesulfonamide

: 53973-85-6
N-Methyl-2-(4-methylphenylsulfonyl)benzolamin

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / KOH / H₂O / 1) 40 degC, 15 min, 2) reflux, 10 min

2: 39 percent / n-BuLi / tetrahydrofuran / -105 degC -> room temp.

With potassium hydroxide; n-butyllithium; In tetrahydrofuran; water;