Phenyl 3-methylbut-2-enoate

Base Information

Chemical Name:Phenyl 3-methylbut-2-enoate
CAS No.:54897-52-8
Molecular Formula:C11H12O2
Molecular Weight:176.215
Hs Code.:
DSSTox Substance ID:DTXSID40339684
Nikkaji Number:J2.861.234F

Synonyms:phenyl 3-methylbut-2-enoate;Phenyl 3,3-dimethylacrylate;54897-52-8;Phenyl 3.3-dimethylacrylate;SCHEMBL1405221;Phenyl 3-methyl-2-butenoate #;DTXSID40339684;AKOS002947419;3-Methyl-2-butenoic acid phenyl ester;3-Methyl-2-butenoic acid, phenyl ester

Suppliers and Price of Phenyl 3-methylbut-2-enoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Phenyl 3-methylbut-2-enoate

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:176.083729621
Heavy Atom Count:13
Complexity:196

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=CC(=O)OC1=CC=CC=C1)C

Technology Process of Phenyl 3-methylbut-2-enoate

There total 13 articles about Phenyl 3-methylbut-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 3350-78-5
3,3-Dimethylacryloyl chloride

: 108-95-2,27073-41-2
phenol

: 54897-52-8
phenyl 3,3-dimethylacrylate

Guidance literature:: phenol; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.25h;

3,3-Dimethylacryloyl chloride; In tetrahydrofuran; at 0 - 20 ℃; for 3h;
DOI:10.1016/j.tetlet.2016.10.005

Reference yield:

: 57539-84-1
1,3-Dichloro-3-methyl-2-butanone

: 108-95-2,27073-41-2
phenol

: 563-80-4
3-methyl-butan-2-one

: 54897-52-8
phenyl 3,3-dimethylacrylate

: 87575-38-0
1-Phenoxy-3-methyl-2-butanone

Guidance literature:: With tetraethylammonium perchlorate; In N,N-dimethyl-formamide; at 20 ℃; mercury pool electrode;

Reference yield:

: 201230-82-2
carbon monoxide

: 563-47-3
3-Chloro-2-methylpropene

: 108-95-2,27073-41-2
phenol

: 54897-52-8
phenyl 3,3-dimethylacrylate

: Phenyl 3-methyl-3-butenoate

Guidance literature:: With palladium diacetate; triethylamine; triphenylphosphine; In tetrahydrofuran; at 100 ℃; for 10h; under 20686.5 Torr; Autoclave;
DOI:10.1055/s-0031-1289659