n-Methyl-n-(1-phenylethyl)aniline

Base Information

• Chemical Name: n-Methyl-n-(1-phenylethyl)aniline
• CAS No.: 6299-04-3
• Molecular Formula: C15H17 N
• Molecular Weight: 211.307
• Hs Code.: 2921430090
• NSC Number: 42455
• DSSTox Substance ID: DTXSID30285601
• Nikkaji Number: J653.140G
• Mol file: 6299-04-3.mol

Synonyms:n-methyl-n-(1-phenylethyl)aniline;6299-04-3;NSC42455;SCHEMBL2232118;DTXSID30285601;NSC-42455

Chemical Property of n-Methyl-n-(1-phenylethyl)aniline

Chemical Property:

• Vapor Pressure: 0.000321mmHg at 25°C
• Boiling Point: 320.3°C at 760 mmHg
• Flash Point: 130.4°C
• PSA: 3.24000
• Density: 1.028g/cm³
• LogP: 3.88400
• XLogP3: 3.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 211.136099547
• Heavy Atom Count: 16
• Complexity: 190

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C1=CC=CC=C1)N(C)C2=CC=CC=C2

Technology Process of n-Methyl-n-(1-phenylethyl)aniline

There total 35 articles about n-Methyl-n-(1-phenylethyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

phenylacetylene (536-74-3) + N-methylaniline (100-61-8) → N-methyl-N-phenylethylaniline (6299-04-3)

Guidance literature:

phenylacetylene; N-methylaniline; With indium(III) bromide; In toluene; at 110 ℃; for 3h; Inert atmosphere;

With Dimethylphenylsilane; In toluene; at 60 ℃; for 30h;

DOI:10.1002/ejoc.201402544

Reference yield: 93.0%

benzylidene phenylamine (538-51-2) + methyl iodide (74-88-4) → N-methyl-N-phenylethylaniline (6299-04-3)

Guidance literature:

With strontium; In tetrahydrofuran; at 20 ℃; for 2h;

DOI:10.1246/cl.2005.760

Reference yield: 92.0%

acetophenone (98-86-2) + N-methylaniline (100-61-8) → N-methyl-N-phenylethylaniline (6299-04-3)

Guidance literature:

acetophenone; N-methylaniline; With N,N,N,N,-tetramethylethylenediamine; In dichloromethane; at 20 ℃; for 0.5h;

With trichlorosilane; In dichloromethane; for 36h;

DOI:10.3390/molecules17055151

upstream raw materials:

N-methyl-N-(1-phenylethenyl)aniline

(1-chloroethyl)benzene

N-methylaniline

benzenediazonium tetrafluoroborate

Downstream raw materials:

N-methyl-N-(1-phenyl-ethyl)-aniline-N-oxide