4-phenylbutyl acetate

Base Information

• Chemical Name: 4-phenylbutyl acetate
• CAS No.: 7492-40-2
• Molecular Formula: C12H16O2
• Molecular Weight: 192.258
• Mol file: 7492-40-2.mol

Synonyms:

Chemical Property of 4-phenylbutyl acetate

Chemical Property:

• Vapor Pressure: 0.00288mmHg at 25°C
• Boiling Point: 285°Cat760mmHg
• Flash Point: 120°C
• Density: 1.002g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-phenylbutyl acetate

There total 15 articles about 4-phenylbutyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-phenyl-butan-1-ol (3360-41-6) + acetic acid (64-19-7,77671-22-8) → 4-phenylbutyl acetate (7492-40-2)

Guidance literature:

With iron(III) chloride; at 20 ℃; for 1h;

DOI:10.1055/s-1999-2806

Reference yield: 96.0%

(4-(benzyloxy)butyl)benzene (101747-16-4) + ethyl acetate (141-78-6) → 4-phenylbutyl acetate (7492-40-2)

Guidance literature:

With Bromotrichloromethane; (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere; Irradiation;

DOI:10.1021/acs.orglett.5b00663

Reference yield: 93.0%

4-phenyl-butan-1-ol (3360-41-6) + acetic anhydride (108-24-7) → 4-phenylbutyl acetate (7492-40-2)

Guidance literature:

With lithium trifluoromethanesulfonate; at 20 ℃; for 15h;

DOI:10.1021/jo026678+

upstream raw materials:

4-phenyl-butan-1-ol

acetic anhydride

4-iodobutyl acetate

acetyl chloride

Downstream raw materials:

1-[4-(4-hydroxy-butyl)-phenyl]-ethanone

4-phenyl-butan-1-ol

4-acetoxy-1-phenylbutyl nitrate

4-Brom-4-phenyl-butylacetat

Refernces

• 1、 Lu, Ping,Hou, Tianyuan,Gu, Xiangyong,Li, Pixu. "Visible-light-promoted conversion of alkyl benzyl ether to alkyl ester or alcohol via O-α-sp3 C-H cleavage". . p. 1954 - 1957. Retrieved 2015/04/27.
• 2、 Zeng, Tieqiang,Song, Gonghua,Li, Chao-Jun. "Separation, recovery and reuse of N-heterocyclic carbene catalysts in transesterification reactions". supporting information; experimental part. p. 6249 - 6251. Retrieved 2010/02/16.