4-BROMO-2-IODOACETANILDE

Base Information

• Chemical Name: 4-BROMO-2-IODOACETANILDE
• CAS No.: 562080-91-5
• Molecular Formula: C8H7BrINO
• Molecular Weight: 339.958
• Hs Code.: 2924299090
• Mol file: 562080-91-5.mol

Synonyms:

Chemical Property of 4-BROMO-2-IODOACETANILDE

Chemical Property:

• PSA: 29.10000
• LogP: 3.08510

Purity/Quality:

99.0% ^*data from raw suppliers

N-(4-Bromo-2-iodophenyl)acetamide 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-BROMO-2-IODOACETANILDE

There total 7 articles about 4-BROMO-2-IODOACETANILDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-bromo-2-iodoaniline (66416-72-6) + acetyl chloride (75-36-5) → N-(4-bromo-2-iodophenyl)acetamide (562080-91-5)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1016/j.tetlet.2018.01.014

Reference yield: 88.5%

4-bromo-2-iodoaniline (66416-72-6) + acetic anhydride (108-24-7) → N-(4-bromo-2-iodophenyl)acetamide (562080-91-5)

Guidance literature:

In dichloromethane; at 20 ℃;

DOI:10.1021/acs.jmedchem.5b00440

Reference yield: 68.0%

4-bromoacetanilide (103-88-8) → N-(4-bromo-2-iodophenyl)acetamide (562080-91-5)

Guidance literature:

With N-iodo-succinimide; cobalt acetylacetonate; trifluoroacetic acid; silver(l) oxide; In 1,2-dichloro-ethane; at 60 ℃; for 16h; regioselective reaction;

DOI:10.1039/c8ob01448e

upstream raw materials:

4-bromo-2-iodoaniline

acetic anhydride

4-bromo-aniline

4-bromoacetanilide

Downstream raw materials:

6-bromo-2-methylbenzothiazole

4-(5-bromo-1H-indol-2-yl)-N-methylbenzenamine

4-(5-bromo-1H-indol-2-yl)-N,N-dimethylbenzenamine

5-bromo-2-(4-methoxyphenyl)-1H-indole

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