Diethyl (1-chloropropyl)phosphonate

Base Information

Chemical Name:Diethyl (1-chloropropyl)phosphonate
CAS No.:56436-86-3
Molecular Formula:C7H16ClO3P
Molecular Weight:214.629
Hs Code.:
DSSTox Substance ID:DTXSID60553582
Nikkaji Number:J336.305H

Synonyms:56436-86-3;Diethyl (1-chloropropyl)phosphonate;DTXSID60553582

Suppliers and Price of Diethyl (1-chloropropyl)phosphonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Diethyl (1-chloropropyl)phosphonate

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:214.0525591
Heavy Atom Count:12
Complexity:153

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC(P(=O)(OCC)OCC)Cl

Technology Process of Diethyl (1-chloropropyl)phosphonate

There total 1 articles about Diethyl (1-chloropropyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64-17-5
ethanol

: 540-54-5
1-Chloropropane

: 40217-77-4
(2-chloro-1-methyl-ethyl)-phosphonic acid diethyl ester

: 23269-98-9
diethyl (3-chloropropyl)phosphonate

: 13674-88-9
3-Chloropropan-2-yl diethyl phosphate

: 56436-86-3
diethyl α-chloropropylphosphonate

Guidance literature:: Multistep reaction; (i) PCl₃, O₂, (ii) /BRN= 1718733/;
DOI:10.1246/bcsj.48.484

Reference yield: 60.0%

: 56436-86-3
diethyl α-chloropropylphosphonate

: 368-47-8
phenyltrifluorosilane

: 33973-50-1
diethyl α-phenylpropylphosphonate

Guidance literature:: With (1,2-dimethoxyethane)dichloronickel(II); (1S,2R)-(+)-norphedrine; lithium hexamethyldisilazane; water; cesium fluoride; In N,N-dimethyl acetamide; at 60 ℃; for 16h;
DOI:10.1002/anie.200700440

Reference yield:

: 56436-86-3
diethyl α-chloropropylphosphonate

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: C₁₉H₂₆O₃P₂

Guidance literature:: diethyl α-chloropropylphosphonate; With n-butyllithium; In tetrahydrofuran; hexane; at -70 ℃; Inert atmosphere;

chloro-diphenylphosphine; In tetrahydrofuran; hexane; for 2h; Inert atmosphere; Reflux;
DOI:10.1016/j.tetlet.2008.07.144