(5α,11S,13β,19α)-1,2-Didehydro-3β-methoxycrinan-11-ol

Base Information

Chemical Name:(5α,11S,13β,19α)-1,2-Didehydro-3β-methoxycrinan-11-ol
CAS No.:1472-76-0
Molecular Formula:C17H19 N O4
Molecular Weight:301.342
Hs Code.:
Mol file:1472-76-0.mol

Synonyms:11-Epihemanthamine(6CI,7CI); Crinan-11-ol, 1,2-didehydro-3-methoxy-, (3b,5a,11S,13b,19a)-; (-)-11-epi-Haemanthamine;11-Epihaemanthamine; 12-Epihemanthamine;3H,6H-5,11b-Ethano[1,3]dioxolo[4,5-j]phenanthridin-12-ol,4,4a-dihydro-3-methoxy-, [3S-(3a,4aa,5b,11bb,12R*)]-

Suppliers and Price of (5α,11S,13β,19α)-1,2-Didehydro-3β-methoxycrinan-11-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of (5α,11S,13β,19α)-1,2-Didehydro-3β-methoxycrinan-11-ol

Chemical Property:

PSA：51.16000
LogP:1.12460

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (5α,11S,13β,19α)-1,2-Didehydro-3β-methoxycrinan-11-ol

There total 13 articles about (5α,11S,13β,19α)-1,2-Didehydro-3β-methoxycrinan-11-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1472-75-9
Oxohaemanthamin

: 466-75-1,639-41-8,1472-76-0,35598-60-8,41855-34-9,60944-30-1
haemanthamine

Guidance literature:: With sodium tetrahydroborate; In methanol;
DOI:10.1021/ja01486a045

Reference yield:

: 466-75-1
haemanthamine

: 466-75-1,639-41-8,1472-76-0,35598-60-8,41855-34-9,60944-30-1
haemanthamine

Guidance literature:: Multi-step reaction with 2 steps

1: CrO₃ / pyridine

2: NaBH₄ / methanol

With chromium(VI) oxide; sodium tetrahydroborate; In pyridine; methanol;
DOI:10.1021/ja01486a045

Reference yield:

: 466-75-1,639-41-8,1472-76-0,35598-60-8,41855-34-9,60944-30-1
haemanthamine

: 466-75-1,639-41-8,1472-76-0,35598-60-8,41855-34-9,60944-30-1
haemanthamine

Guidance literature:: Multi-step reaction with 2 steps

1: CrO₃; pyridine

2: NaBH₄ / methanol

With pyridine; chromium(VI) oxide; sodium tetrahydroborate; In methanol;
DOI:10.1021/ja01486a045