5-Methoxy-2-methylbenzaldehyde

Base Information

• Chemical Name: 5-Methoxy-2-methylbenzaldehyde
• CAS No.: 56724-09-5
• Molecular Formula: C9H10O2
• Molecular Weight: 150.177
• European Community (EC) Number: 854-710-8
• DSSTox Substance ID: DTXSID20492928
• Nikkaji Number: J1.782.482A
• Wikidata: Q82339166

Synonyms:5-Methoxy-2-methylbenzaldehyde;56724-09-5;MFCD12547802;2-methyl-5-methoxybenzaldehyde;6-Methyl-m-anisaldehyde;SCHEMBL2505574;5-methoxy-2-methyl-benzaldehyde;DTXSID20492928;ZCEYVMICIGLTMC-UHFFFAOYSA-N;AKOS006346091;SB74673;AS-33058;SY104408;CS-0061328;EN300-1168253;A856524;Z1201626604

Chemical Property of 5-Methoxy-2-methylbenzaldehyde

Chemical Property:

• PSA: 26.30000
• LogP: 1.81610
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C
• XLogP3: 2.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 150.068079557
• Heavy Atom Count: 11
• Complexity: 134

Purity/Quality:

97% ^*data from raw suppliers

5-methoxy-2-methylbenzaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C=C(C=C1)OC)C=O

Technology Process of 5-Methoxy-2-methylbenzaldehyde

There total 32 articles about 5-Methoxy-2-methylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

Trimethylboroxine (823-96-1) + 2-bromo-5-methoxy-benzaldehyde (7507-86-0) → 5-methoxy-2-methylbenzaldehyde (56724-09-5)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,4-dioxane; for 23h; Reflux;

Reference yield: 89.0%

(5-methoxy-2-methylphenyl)methanol (73502-04-2) → 5-methoxy-2-methylbenzaldehyde (56724-09-5)

Guidance literature:

(5-methoxy-2-methylphenyl)methanol; With oxalyl dichloride; In dichloromethane; dimethyl sulfoxide; at -78 ℃; for 1h;

With triethylamine; In dichloromethane; dimethyl sulfoxide; at -78 - 20 ℃; for 3h; Inert atmosphere;

DOI:10.1016/j.bmcl.2016.01.067

Reference yield: 88.0%

2-(5-methoxy-2-methylphenyl)-[1,3]dioxolane (170282-84-5) → 5-methoxy-2-methylbenzaldehyde (56724-09-5)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; for 48h;

upstream raw materials:

5-methoxy-2-methyl-benzoyl chloride

(4-Methoxy-benzyl)-dimethyl-phenylsulfanylmethyl-ammonium; chloride

N,N-dimethyl-4-methoxylbenzylamine

(5-methoxy-2-methylphenyl)methanol

Downstream raw materials:

2-Nitro-3-methoxy-6-methyl-benzaldehyd

(5-methoxy-2-methylphenyl)methanol

C₁₈H₂₂O₂

C₂₀H₂₆O₂

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