2,5-Dimethoxy-3-nitroaniline

Base Information

Chemical Name:2,5-Dimethoxy-3-nitroaniline
CAS No.:56741-29-8
Molecular Formula:C8H10N2O4
Molecular Weight:198.178
Hs Code.:
DSSTox Substance ID:DTXSID90453001
Wikidata:Q82273960

Synonyms:2,5-dimethoxy-3-nitroaniline;56741-29-8;Benzenamine, 2,5-dimethoxy-3-nitro-;SCHEMBL9138248;DTXSID90453001;SB76752;InChI=1/C8H10N2O4/c1-13-5-3-6(9)8(14-2)7(4-5)10(11)12/h3-4H,9H2,1-2H

Suppliers and Price of 2,5-Dimethoxy-3-nitroaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2,5-Dimethoxy-3-nitroaniline

Chemical Property:

Melting Point:87.5-89.5 °C(Solv: benzene (71-43-2); isooctane (540-84-1))
Boiling Point:401.1±40.0 °C(Predicted)
PSA：90.30000
Density:1.307±0.06 g/cm3(Predicted)
LogP:2.29860
XLogP3:1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:2
Exact Mass:198.06405680
Heavy Atom Count:14
Complexity:206

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=C(C(=C1)[N+](=O)[O-])OC)N

Technology Process of 2,5-Dimethoxy-3-nitroaniline

There total 8 articles about 2,5-Dimethoxy-3-nitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 15174-07-9
1,4-dimethoxy-2,6-dinitrobenzene

: 56741-29-8
2,5-dimethoxy-3-nitroaniline

Guidance literature:: With palladium 10% on activated carbon; cyclohexene; In ethanol; at 45 ℃; for 5h;
DOI:10.1002/ejoc.201100131

Reference yield:

: 3410-94-4
4-methoxy-2,6-dinitrophenol

: 56741-29-8
2,5-dimethoxy-3-nitroaniline

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / diethyl ether

2: cyclohexene / palladium on carbon / ethanol / 0.25 h / Heating

With cyclohexene; palladium on activated charcoal; In diethyl ether; ethanol;
DOI:10.1021/jo7017813

Reference yield:

: 1568-70-3
4-methoxy-2-nitrophenol

: 56741-29-8
2,5-dimethoxy-3-nitroaniline

Guidance literature:: Multi-step reaction with 3 steps

1: 21 g / glacial acetic acid; nitric acid / 15 - 30 °C

2: 99 percent / diethyl ether

3: cyclohexene / palladium on carbon / ethanol / 0.25 h / Heating

With nitric acid; acetic acid; cyclohexene; palladium on activated charcoal; In diethyl ether; ethanol;
DOI:10.1021/jo7017813