Benzoic acid, 2,4,6-tris(1-methylethyl)-, methyl ester

Base Information

Chemical Name:Benzoic acid, 2,4,6-tris(1-methylethyl)-, methyl ester
CAS No.:57198-98-8
Molecular Formula:C17H26O2
Molecular Weight:262.392
Hs Code.:

Synonyms:methyl 2,4,6-triisopropylbenzoate;2,4,6-triisopropyl-benzoic acid methyl ester;2,4,6-Triisopropyl-benzoesaeure-methylester;Methyl-2,4,6-triisopropylbenzoat;

Suppliers and Price of Benzoic acid, 2,4,6-tris(1-methylethyl)-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 2,4,6-tris(1-methylethyl)-, methyl ester

Chemical Property:

PSA：26.30000
LogP:4.84340

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 2,4,6-tris(1-methylethyl)-, methyl ester

There total 11 articles about Benzoic acid, 2,4,6-tris(1-methylethyl)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 49623-71-4
2,4,6-triisopropylbenzoic acid

: 74-89-5
methylamine

: 57198-98-8
methyl 2,4,6-triisopropylbenzoate

Guidance literature:: With propane-1,3-diyl dinitrite; In tetrahydrofuran; at 90 ℃; for 0.333333h; under 12929 Torr; Flow reactor;
DOI:10.1021/acs.orglett.7b02231

Reference yield: 60.0%

: 75-15-0,12122-00-8
carbon disulfide

: 111-71-7
heptanal

: 63846-79-7
(tributylstannyl)methyl 2,4,6-triisopropylbenzoate

: 74-88-4
methyl iodide

: 1133931-99-3
S-methyl O-[1-hexyl-2-(2,4,6-triisopropylbenzoyloxy)ethyl] dithiocarbonate

: 57198-98-8
methyl 2,4,6-triisopropylbenzoate

Guidance literature:: (tributylstannyl)methyl 2,4,6-triisopropylbenzoate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.0833333h; Inert atmosphere;

heptanal; In tetrahydrofuran; hexane; at -78 ℃; for 0.166667h; Inert atmosphere;

carbon disulfide; methyl iodide; Further stages;
DOI:10.1021/jo802625q

Reference yield: 55.0%

: 75-15-0,12122-00-8
carbon disulfide

: 111-71-7
heptanal

: 1133931-84-6,1133931-83-5
C₂₉H₅₁⁽²⁾HO₂Sn

: 74-88-4
methyl iodide

: C₂₆H₄₁⁽²⁾HO₃S₂

: 1133932-00-9
C₂₆H₄₁⁽²⁾HO₃S₂

: 57198-98-8
methyl 2,4,6-triisopropylbenzoate

Guidance literature:: C₂₉H₅₁⁽²⁾HO₂Sn; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.0833333h; Inert atmosphere;

heptanal; In tetrahydrofuran; hexane; at -78 ℃; for 0.166667h; Inert atmosphere;

carbon disulfide; methyl iodide; optical yield given as %ee; Further stages;
DOI:10.1021/jo802625q