1H-Pyrrole, 1-ethenyl-3-methyl-2-phenyl-

Base Information

Chemical Name:1H-Pyrrole, 1-ethenyl-3-methyl-2-phenyl-
CAS No.:57807-57-5
Molecular Formula:C13H13N
Molecular Weight:183.253
Hs Code.:
DSSTox Substance ID:DTXSID00394077

Synonyms:1H-Pyrrole, 1-ethenyl-3-methyl-2-phenyl-;57807-57-5;DTXSID00394077;1-vinyl-2-phenyl-3-methylpyrrole;AKOS024359506;InChI=1/C13H13N/c1-3-14-10-9-11(2)13(14)12-7-5-4-6-8-12/h3-10H,1H2,2H

Suppliers and Price of 1H-Pyrrole, 1-ethenyl-3-methyl-2-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 1H-Pyrrole, 1-ethenyl-3-methyl-2-phenyl-

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:183.104799419
Heavy Atom Count:14
Complexity:193

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(N(C=C1)C=C)C2=CC=CC=C2

Technology Process of 1H-Pyrrole, 1-ethenyl-3-methyl-2-phenyl-

There total 4 articles about 1H-Pyrrole, 1-ethenyl-3-methyl-2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 2157-50-8
propiophenone oxime

: 75-20-7
calcium carbide

: 20814-35-1
3-methyl-2-phenyl-1H-pyrrole

: 57807-57-5
3-methyl-2-phenyl-1-vinyl-pyrrole

Guidance literature:: With 18-crown-6 ether; water; potassium hydroxide; In dimethyl sulfoxide; at 100 ℃; for 15h; Sealed tube; Green chemistry;
DOI:10.1039/c4gc01615g

Reference yield: 10.0%

: 2157-50-8
propiophenone oxime

: 74-86-2,25067-58-7
acetylene

: 20814-35-1
3-methyl-2-phenyl-1H-pyrrole

: 57807-57-5
3-methyl-2-phenyl-1-vinyl-pyrrole

Guidance literature:: With potassium hydroxide; In dimethyl sulfoxide; at 50 - 60 ℃; for 3h; under 9120 - 10640 Torr; Yields of byproduct given;
DOI:10.1007/BF00515220

Reference yield:

: 93-55-0
1-phenyl-propan-1-one

: 20814-35-1
3-methyl-2-phenyl-1H-pyrrole

: 57807-57-5
3-methyl-2-phenyl-1-vinyl-pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride

2: water; potassium hydroxide; 18-crown-6 ether / dimethyl sulfoxide / 15 h / 100 °C / Sealed tube; Green chemistry

With 18-crown-6 ether; hydroxylamine hydrochloride; water; potassium hydroxide; In dimethyl sulfoxide;
DOI:10.1039/c4gc01615g