3-(4-Methoxyphenyl)-1lambda~6~,2,4-benzothiadiazine-1,1(4H)-dione

Base Information

Chemical Name:3-(4-Methoxyphenyl)-1lambda~6~,2,4-benzothiadiazine-1,1(4H)-dione
CAS No.:57864-70-7
Molecular Formula:C14H12N2O3S
Molecular Weight:288.327
Hs Code.:
DSSTox Substance ID:DTXSID70506529
Nikkaji Number:J3.027.063K
Wikidata:Q82362310

Synonyms:57864-70-7;DTXSID70506529;3-(4-Methoxyphenyl)-1lambda~6~,2,4-benzothiadiazine-1,1(4H)-dione;AKOS032951607

Suppliers and Price of 3-(4-Methoxyphenyl)-1lambda~6~,2,4-benzothiadiazine-1,1(4H)-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 3-(4-Methoxyphenyl)-1lambda~6~,2,4-benzothiadiazine-1,1(4H)-dione

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:288.05686342
Heavy Atom Count:20
Complexity:475

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C2=NS(=O)(=O)C3=CC=CC=C3N2

Technology Process of 3-(4-Methoxyphenyl)-1lambda~6~,2,4-benzothiadiazine-1,1(4H)-dione

There total 10 articles about 3-(4-Methoxyphenyl)-1lambda~6~,2,4-benzothiadiazine-1,1(4H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 123-11-5
4-methoxy-benzaldehyde

: 3306-62-5
2-AMINOBENZENESULFONAMIDE

: 57864-70-7
3-(4-methoxyphenyl)-2H-benzo[e][1,2,4]thiadiazine 1,1-dioxide

Guidance literature:: With sodium hydrogensulfite; In N,N-dimethyl acetamide; at 150 ℃; for 2h;
DOI:10.1055/s-1981-29322

Reference yield: 89.0%

: 100-09-4
4-methoxybenzoic acid

: 3306-62-5
2-AMINOBENZENESULFONAMIDE

: 57864-70-7
3-(4-methoxy-phenyl)-4H-benzo[e][1,2,4]thiadiazine 1,1-dioxide

Guidance literature:: With polyphosphoric acid trimethylsilyl ester; at 160 ℃; for 2h;
DOI:10.1055/s-1983-30543

Reference yield: 87.0%

: 3306-62-5
2-AMINOBENZENESULFONAMIDE

: 105-13-5
4-Methoxybenzyl alcohol

: 57864-70-7
3-(4-methoxyphenyl)-2H-benzo[e][1,2,4]thiadiazine 1,1-dioxide

Guidance literature:: With but-2-enenitrile; carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II); 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In toluene; at 115 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c1ob06516e