6-Chloro-6-deoxygalactose

Base Information

• Chemical Name: 6-Chloro-6-deoxygalactose
• CAS No.: 18465-32-2
• Molecular Formula: C₆H₁₁ClO₅
• Molecular Weight: 198.603
• DSSTox Substance ID: DTXSID20171605
• Wikidata: Q83041691
• Mol file: 18465-32-2.mol

Synonyms:6-chloro-6-deoxygalactose;6-chloro-6-deoxygalactose, (L)-isomer

Chemical Property of 6-Chloro-6-deoxygalactose

Chemical Property:

• Vapor Pressure: 5.97E-11mmHg at 25°C
• Boiling Point: 473.4°Cat760mmHg
• Flash Point: 240.1°C
• PSA: 97.99000
• Density: 1.553g/cm³
• LogP: -2.13230
• XLogP3: -1.7
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 5
• Exact Mass: 198.0295011
• Heavy Atom Count: 12
• Complexity: 142

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(C(C(C(C(C=O)O)O)O)O)Cl
• Isomeric SMILES: C([C@H]([C@@H]([C@@H]([C@H](C=O)O)O)O)O)Cl

Technology Process of 6-Chloro-6-deoxygalactose

There total 7 articles about 6-Chloro-6-deoxygalactose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

methyl 6-chloro-6-deoxy-β-D-glucopyranoside (4990-84-5) → 6-chloro-6-deoxy-D-glucose (40656-44-8,18465-32-2)

Guidance literature:

With sulfuric acid;

DOI:10.1016/S0008-6215(00)90022-3

Reference yield: 35.0%

6-chloro-6-deoxy-glucose tetraacetate + D-glucose (50-99-7) + methanesulfonyl chloride (124-63-0) → 6-chloro-6-deoxy-D-glucose (40656-44-8,18465-32-2)

Guidance literature:

With sodium methylate; acetic anhydride; In pyridine; methanol; ethanol; water; N,N-dimethyl-formamide;

Reference yield:

→ 6-chloro-6-deoxy-D-glucose (40656-44-8,18465-32-2)

Guidance literature:

With hydrogenchloride;

upstream raw materials:

6-chloro-O¹,O²;O³,O⁵-diisopropylidene-α-D-6-deoxy-glucofuranose

methyl 6-chloro-6-deoxy-β-D-glucopyranoside

D-glucose

methanesulfonyl chloride

Downstream raw materials:

6-chloro-D-arabino-6-deoxy-[2]hexosulose-bis-phenylhydrazone

6-chloro-6-deoxy-D-glucitol

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