1-(4-PYRROL-1-YL-PHENYL)-ETHANONE

Base Information

• Chemical Name: 1-(4-PYRROL-1-YL-PHENYL)-ETHANONE
• CAS No.: 22106-37-2
• Molecular Formula: C12H11NO
• Molecular Weight: 185.225
• Hs Code.: 2933990090
• Mol file: 22106-37-2.mol

Synonyms:Acetophenone,4'-pyrrol-1-yl- (8CI);1-(p-Acetylphenyl)pyrrole;N-(4-Acetylphenyl)pyrrole;1-[4-(1H-Pyrrol-1-yl)phenyl]ethanone;1-(4-Pyrrol-1-yl-phenyl)-ethanone;

Chemical Property of 1-(4-PYRROL-1-YL-PHENYL)-ETHANONE

Chemical Property:

• Vapor Pressure: 0.000311mmHg at 25°C
• Refractive Index: 1.565
• Boiling Point: 320.8 °C at 760 mmHg
• Flash Point: 147.8 °C
• PSA: 22.00000
• Density: 1.05 g/cm³
• LogP: 2.67990

Purity/Quality:

99%, ^*data from raw suppliers

1-[4-(1H-pyrrol-1-yl)phenyl]ethanone ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(4-PYRROL-1-YL-PHENYL)-ETHANONE

There total 14 articles about 1-(4-PYRROL-1-YL-PHENYL)-ETHANONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

pyrrole (109-97-7,30604-81-0) + 4-Iodoacetophenone (13329-40-3) → 4-(1H-pyrrol-1-yl)acetophenone (22106-37-2)

Guidance literature:

With copper(II) acetate monohydrate; caesium carbonate; In N,N-dimethyl-formamide; at 110 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.tet.2011.05.025

Reference yield: 89.0%

cis,trans-2,5-dimethoxytetrahydrofuran (696-59-3) + p-aminobenzophenone (99-92-3) → 4-(1H-pyrrol-1-yl)acetophenone (22106-37-2)

Guidance literature:

With ionic liquid immobilized on γ-Fe₂O₃(at)SiO₂ nanoparticles; In water; at 100 ℃; for 0.833333h;

DOI:10.1016/j.apcata.2013.03.005

Reference yield: 88.0%

cis,trans-2,5-dimethoxytetrahydrofuran (696-59-3) + (4-nitrophenyl)ethanone (100-19-6) → 4-(1H-pyrrol-1-yl)acetophenone (22106-37-2)

Guidance literature:

With hydrogen; In neat (no solvent); at 120 ℃; for 24h; under 30003 Torr; Autoclave; Green chemistry;

DOI:10.1002/anie.202007613

upstream raw materials:

cis,trans-2,5-dimethoxytetrahydrofuran

p-aminobenzophenone

pyrrole

para-chloroacetophenone

Downstream raw materials:

1-[4-(pyrrol-1-yl)phenyl]-3-(pyrrol-2-yl)prop-2-en-1-one

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