Benzenamine, N-[[bis(phenylmethyl)phosphinyl]methyl]-

Base Information

Chemical Name:Benzenamine, N-[[bis(phenylmethyl)phosphinyl]methyl]-
CAS No.:59170-69-3
Molecular Formula:C21H22NOP
Molecular Weight:335.386
Hs Code.:
DSSTox Substance ID:DTXSID60364094
Wikidata:Q82147863

Synonyms:59170-69-3;Dibenzyl((phenylamino)methyl)phosphine oxide;Benzenamine, N-[[bis(phenylmethyl)phosphinyl]methyl]-;DTXSID60364094

Suppliers and Price of Benzenamine, N-[[bis(phenylmethyl)phosphinyl]methyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenamine, N-[[bis(phenylmethyl)phosphinyl]methyl]-

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:7
Exact Mass:335.143901323
Heavy Atom Count:24
Complexity:369

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CP(=O)(CC2=CC=CC=C2)CNC3=CC=CC=C3

Technology Process of Benzenamine, N-[[bis(phenylmethyl)phosphinyl]methyl]-

There total 5 articles about Benzenamine, N-[[bis(phenylmethyl)phosphinyl]methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 13238-16-9
dibenzylphosphine oxide

: 62-53-3
aniline

: 59170-69-3
(phenylaminomethyl)dibenzylphosphine oxide

Guidance literature:: In acetonitrile; at 100 ℃; for 1h; Microwave irradiation; Sealed tube;
DOI:10.1016/j.jorganchem.2015.10.029

Reference yield:

: 100-39-0
benzyl bromide

: 59170-69-3
(phenylaminomethyl)dibenzylphosphine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: phosphonic acid diethyl ester; magnesium / diethyl ether / 1.5 h / 25 °C

2: acetonitrile / 1 h / 100 °C / Microwave irradiation; Sealed tube

With magnesium; phosphonic acid diethyl ester; In diethyl ether; acetonitrile; 2: |Kabachnik-Fields Reaction;
DOI:10.1016/j.jorganchem.2015.10.029